5,6,7,8-tetradeoxy-5,8-(N-benzylimino)-1,2-O-isopropylidene-α-D-gluco-octo-1,4-furanose

Base Information

Chemical Name:5,6,7,8-tetradeoxy-5,8-(N-benzylimino)-1,2-O-isopropylidene-α-D-gluco-octo-1,4-furanose
CAS No.:887239-58-9
Molecular Formula:C₂₅H₃₁NO₄
Molecular Weight:409.525
Hs Code.:

Synonyms:5,6,7,8-tetradeoxy-5,8-(N-benzylimino)-1,2-O-isopropylidene-α-D-gluco-octo-1,4-furanose

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Chemical Property of 5,6,7,8-tetradeoxy-5,8-(N-benzylimino)-1,2-O-isopropylidene-α-D-gluco-octo-1,4-furanose

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Technology Process of 5,6,7,8-tetradeoxy-5,8-(N-benzylimino)-1,2-O-isopropylidene-α-D-gluco-octo-1,4-furanose

There total 1 articles about 5,6,7,8-tetradeoxy-5,8-(N-benzylimino)-1,2-O-isopropylidene-α-D-gluco-octo-1,4-furanose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 690981-92-1
3-O-benzyl-1,2-O-isopropylidene-5,6,7,8-tetradeoxy-5-N-(benzylamino)-α-D-gluco-7-eno-octo-1,4-furanose

: 887239-58-9
5,6,7,8-tetradeoxy-5,8-(N-benzylimino)-1,2-O-isopropylidene-α-D-gluco-octo-1,4-furanose

Guidance literature:: 3-O-benzyl-1,2-O-isopropylidene-5,6,7,8-tetradeoxy-5-N-(benzylamino)-α-D-gluco-7-eno-octo-1,4-furanose; With mercury(II) diacetate; In tetrahydrofuran; water; at 20 ℃; for 18h;

With sodium tetrahydroborate; In tetrahydrofuran; water;
DOI:10.3390/10080893

Reference yield:

: 887239-58-9
5,6,7,8-tetradeoxy-5,8-(N-benzylimino)-1,2-O-isopropylidene-α-D-gluco-octo-1,4-furanose

: 115438-58-9
(R)-2-((2R,3R,4R,5S)-3,4,5-Trihydroxy-tetrahydro-furan-2-yl)-pyrrolidine-1-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / Pd-C / methanol / 16 h / 20 °C / 4137.18 Torr

2: 0.13 g / aq. NaHCO₃ / ethanol / 2 h / 25 °C

3: aq. TFA / 2 h / 25 °C

With hydrogen; sodium hydrogencarbonate; trifluoroacetic acid; palladium on activated charcoal; In methanol; ethanol;
DOI:10.3390/10080893

Reference yield:

: 887239-58-9
5,6,7,8-tetradeoxy-5,8-(N-benzylimino)-1,2-O-isopropylidene-α-D-gluco-octo-1,4-furanose

: 115649-93-9
1-deoxy-castanospermine

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / Pd-C / methanol / 16 h / 20 °C / 4137.18 Torr

2: 0.13 g / aq. NaHCO₃ / ethanol / 2 h / 25 °C

3: aq. TFA / 2 h / 25 °C

4: 0.04 g / H₂ / Pd-C / methanol / 16 h / 25 °C / 4137.18 Torr

With hydrogen; sodium hydrogencarbonate; trifluoroacetic acid; palladium on activated charcoal; In methanol; ethanol;
DOI:10.3390/10080893