(2S,3R,4S,5R)-5-(azidomethyl)-4-(benzyloxy)-2-(trityloxymethyl)tetrahydrofuran-3-ol

Base Information

Chemical Name:(2S,3R,4S,5R)-5-(azidomethyl)-4-(benzyloxy)-2-(trityloxymethyl)tetrahydrofuran-3-ol
CAS No.:1190850-90-8
Molecular Formula:C₃₂H₃₁N₃O₄
Molecular Weight:521.616
Hs Code.:

Synonyms:(2S,3R,4S,5R)-5-(azidomethyl)-4-(benzyloxy)-2-(trityloxymethyl)tetrahydrofuran-3-ol

Suppliers and Price of (2S,3R,4S,5R)-5-(azidomethyl)-4-(benzyloxy)-2-(trityloxymethyl)tetrahydrofuran-3-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R,4S,5R)-5-(azidomethyl)-4-(benzyloxy)-2-(trityloxymethyl)tetrahydrofuran-3-ol

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Technology Process of (2S,3R,4S,5R)-5-(azidomethyl)-4-(benzyloxy)-2-(trityloxymethyl)tetrahydrofuran-3-ol

There total 1 articles about (2S,3R,4S,5R)-5-(azidomethyl)-4-(benzyloxy)-2-(trityloxymethyl)tetrahydrofuran-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 898225-39-3
2,5-anhydro-6-azido-4-O-benzyl-6-deoxy-D-glucitol

: 76-83-5
trityl chloride

: 1190850-90-8
(2S,3R,4S,5R)-5-(azidomethyl)-4-(benzyloxy)-2-(trityloxymethyl)tetrahydrofuran-3-ol

Guidance literature:: With pyridine; at 0 ℃; for 18h;
DOI:10.1002/ejoc.200900460

Reference yield: 93.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1190850-90-8
(2S,3R,4S,5R)-5-(azidomethyl)-4-(benzyloxy)-2-(trityloxymethyl)tetrahydrofuran-3-ol

: 1190850-91-9
tert-butyl [(2R,3S,4R,5S)-3-(benzyloxy)-4-hydroxy-5-(trityloxymethyl)tetrahydrofuran-2-yl]methylcarbamate

Guidance literature:: (2S,3R,4S,5R)-5-(azidomethyl)-4-(benzyloxy)-2-(trityloxymethyl)tetrahydrofuran-3-ol; With trimethylphosphane; In tetrahydrofuran; toluene; at 0 ℃; for 1h; Inert atmosphere;

With water; In tetrahydrofuran; toluene; for 6h;

di-tert-butyl dicarbonate; With N-ethyl-N,N-diisopropylamine; In toluene; at 20 ℃; for 12h;
DOI:10.1002/ejoc.200900460