3-(toluene-4-sulfonylamino)-propane-1-sulfonic acid 2,2-dimethyl-propyl ester

Base Information

Chemical Name:3-(toluene-4-sulfonylamino)-propane-1-sulfonic acid 2,2-dimethyl-propyl ester
CAS No.:622405-56-5
Molecular Formula:C₁₅H₂₅NO₅S₂
Molecular Weight:363.499
Hs Code.:

Synonyms:3-(toluene-4-sulfonylamino)-propane-1-sulfonic acid 2,2-dimethyl-propyl ester

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Chemical Property of 3-(toluene-4-sulfonylamino)-propane-1-sulfonic acid 2,2-dimethyl-propyl ester

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Technology Process of 3-(toluene-4-sulfonylamino)-propane-1-sulfonic acid 2,2-dimethyl-propyl ester

There total 1 articles about 3-(toluene-4-sulfonylamino)-propane-1-sulfonic acid 2,2-dimethyl-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 98-59-9
p-toluenesulfonyl chloride

: 3-amino-propane-1-sulfonic acid 2,2-dimethyl-propyl ester; hydrochloride

: 622405-56-5
3-(toluene-4-sulfonylamino)-propane-1-sulfonic acid 2,2-dimethyl-propyl ester

Guidance literature:: With triethylamine; In tetrahydrofuran; water;
DOI:10.1021/ol035323p

Reference yield: 40.0%

: 66074-67-7
9-acridinecarbonyl chloride

: 622405-56-5
3-(toluene-4-sulfonylamino)-propane-1-sulfonic acid 2,2-dimethyl-propyl ester

: 622405-57-6
3-[(acridine-9-carbonyl)-(toluene-4-sulfonyl)-amino]-propane-1-sulfonic acid 2,2-dimethyl-propyl ester

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran;
DOI:10.1021/ol035323p

Reference yield:

: 622405-56-5
3-(toluene-4-sulfonylamino)-propane-1-sulfonic acid 2,2-dimethyl-propyl ester

: 622405-59-8
C₃₄H₄₀N₂O₈S₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: 40 percent / t-BuOK / tetrahydrofuran

2.1: 2,6-di-tert-butyl-4-methylpyridine

2.2: 87 percent / aq. HCl

With 2,6-di-tert-butyl-4-methylpyridine; potassium tert-butylate; In tetrahydrofuran;
DOI:10.1021/ol035323p