(N,N'-bis(2,6-diisopropylphenyl)-3,5-dimethyl-β-diketiminate)Nb(N^tBu)(N(2,6-diisopropylphenyl))

Base Information

• Chemical Name: (N,N'-bis(2,6-diisopropylphenyl)-3,5-dimethyl-β-diketiminate)Nb(N^tBu)(N(2,6-diisopropylphenyl))
• CAS No.: 1566527-00-1
• Molecular Formula: C₄₅H₆₇N₄Nb
• Molecular Weight: 756.96

Synonyms:(N,N'-bis(2,6-diisopropylphenyl)-3,5-dimethyl-β-diketiminate)Nb(N^tBu)(N(2,6-diisopropylphenyl))

Chemical Property of (N,N'-bis(2,6-diisopropylphenyl)-3,5-dimethyl-β-diketiminate)Nb(N^tBu)(N(2,6-diisopropylphenyl))

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Technology Process of (N,N'-bis(2,6-diisopropylphenyl)-3,5-dimethyl-β-diketiminate)Nb(N^tBu)(N(2,6-diisopropylphenyl))

There total 1 articles about (N,N'-bis(2,6-diisopropylphenyl)-3,5-dimethyl-β-diketiminate)Nb(N^tBu)(N(2,6-diisopropylphenyl)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

(monoazabutadiene)Nb(NtBu)(NiPr(2,6-diisopropylphenyl))(THF) (1239665-21-4) + 2,6-diisopropyl-1-azidobenzene (136551-45-6) → bis(2,6-diisopropyl)azobenzene (74685-83-9) + (N,N'-bis(2,6-diisopropylphenyl)-3,5-dimethyl-β-diketiminate)Nb(NtBu)(N(2,6-diisopropylphenyl)) (1566527-00-1) + (tBuN-(C(Me)(CH)C(Me))-N(2,6-diisopropylphenyl))Nb(N(2,6-diisopropylphenyl))2 (1566527-01-2)

Guidance literature:

In benzene; at 55 ℃; for 24h; Inert atmosphere;

DOI:10.1021/ja413194z

Reference yield: 60.0%

Cyclohexyl isocyanide (931-53-3) + (N,N'-bis(2,6-diisopropylphenyl)-3,5-dimethyl-β-diketiminate)Nb(NtBu)(N(2,6-diisopropylphenyl)) (1566527-00-1) → C54H80N5Nb

Guidance literature:

In toluene; for 15h; Inert atmosphere; Schlenk technique; Reflux;

DOI:10.1021/jacs.5b11287

Reference yield: 53.0%

carbon dioxide (124-38-9,18923-20-1) + (N,N'-bis(2,6-diisopropylphenyl)-3,5-dimethyl-β-diketiminate)Nb(NtBu)(N(2,6-diisopropylphenyl)) (1566527-00-1) → (N,N'-bis(2,6-diisopropylphenyl)-3,5-dimethyl-β-diketiminate)Nb(N(2,6-diisopropylphenyl))(N(tBu)CO2)

Guidance literature:

In hexane; at 25 ℃; for 0.166667h; under 760.051 Torr; Schlenk technique;

DOI:10.1039/d0sc03489d

upstream raw materials:

(monoazabutadiene)Nb(N^tBu)(N^iPr(2,6-diisopropylphenyl))(THF)

2,6-diisopropyl-1-azidobenzene

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