C₂₉H₄₀O₄Si

Base Information

Chemical Name:C₂₉H₄₀O₄Si
CAS No.:1391927-63-1
Molecular Formula:C₂₉H₄₀O₄Si
Molecular Weight:480.72
Hs Code.:

C<sub>29</sub>H<sub>40</sub>O<sub>4</sub>Si

Synonyms:C₂₉H₄₀O₄Si

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Chemical Property of C₂₉H₄₀O₄Si

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Technology Process of C₂₉H₄₀O₄Si

There total 8 articles about C₂₉H₄₀O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1391927-45-9
C₃₇H₄₈O₅Si

: 1391927-63-1
C₂₉H₄₀O₄Si

Guidance literature:: With water; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 0 ℃; for 3h;
DOI:10.1021/ol301795a

Reference yield:

: 92512-41-9
C₂₁H₂₈O₃Si

: 1391927-63-1
C₂₉H₄₀O₄Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydride / tetrahydrofuran / 0.33 h / 0 °C / Inert atmosphere

1.2: 2 h / 0 - 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.75 h / -78 - -55 °C / Inert atmosphere

2.2: 0.5 h / -78 °C / Inert atmosphere

2.3: 0.33 h / -78 °C / Inert atmosphere

3.1: N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / dichloromethane / 5 h / 20 °C / Inert atmosphere

4.1: pyridinium p-toluenesulfonate / methanol / 22 h / 40 °C / Inert atmosphere

5.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0.5 h / 20 °C / Molecular sieve; Inert atmosphere

6.1: tetrahydrofuran / -78 °C / Inert atmosphere

6.2: 1 h / 20 °C / Molecular sieve; Inert atmosphere

7.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 3 h / 0 °C

With n-butyllithium; tetrapropylammonium perruthennate; water; pyridinium p-toluenesulfonate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; sodium hydride; 4-methylmorpholine N-oxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; methanol; hexane; dichloromethane;
DOI:10.1021/ol301795a

Reference yield:

: 1391927-39-1
C₂₉H₃₆O₄Si

: 1391927-63-1
C₂₉H₄₀O₄Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.75 h / -78 - -55 °C / Inert atmosphere

1.2: 0.5 h / -78 °C / Inert atmosphere

1.3: 0.33 h / -78 °C / Inert atmosphere

2.1: N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / dichloromethane / 5 h / 20 °C / Inert atmosphere

3.1: pyridinium p-toluenesulfonate / methanol / 22 h / 40 °C / Inert atmosphere

4.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0.5 h / 20 °C / Molecular sieve; Inert atmosphere

5.1: tetrahydrofuran / -78 °C / Inert atmosphere

5.2: 1 h / 20 °C / Molecular sieve; Inert atmosphere

6.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 3 h / 0 °C

With n-butyllithium; tetrapropylammonium perruthennate; water; pyridinium p-toluenesulfonate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; 4-methylmorpholine N-oxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; methanol; hexane; dichloromethane;
DOI:10.1021/ol301795a