(S_S,2R,3S)-N-tert-butanesulfinyl-O-[(tert-butyloxy)carbonyl]-3-phenylisoserine

Base Information

Chemical Name:(S_S,2R,3S)-N-tert-butanesulfinyl-O-[(tert-butyloxy)carbonyl]-3-phenylisoserine
CAS No.:878395-87-0
Molecular Formula:C₁₈H₂₇NO₆S
Molecular Weight:385.481
Hs Code.:

(S<sub>S</sub>,2R,3S)-N-tert-butanesulfinyl-O-[(tert-butyloxy)carbonyl]-3-phenylisoserine

Synonyms:(S_S,2R,3S)-N-tert-butanesulfinyl-O-[(tert-butyloxy)carbonyl]-3-phenylisoserine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S_S,2R,3S)-N-tert-butanesulfinyl-O-[(tert-butyloxy)carbonyl]-3-phenylisoserine

Chemical Property:

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Technology Process of (S_S,2R,3S)-N-tert-butanesulfinyl-O-[(tert-butyloxy)carbonyl]-3-phenylisoserine

There total 3 articles about (S_S,2R,3S)-N-tert-butanesulfinyl-O-[(tert-butyloxy)carbonyl]-3-phenylisoserine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 878395-96-1
(S_S,2R,3S)-N-tert-butanesulfinyl-O-[(tert-butyloxy)carbonyl]-3-phenylisoserine benzyl ester

: 878395-87-0
(S_S,2R,3S)-N-tert-butanesulfinyl-O-[(tert-butyloxy)carbonyl]-3-phenylisoserine

Guidance literature:: With hydrogen; palladium dihydroxide; In methanol; for 12h; under 760 Torr;
DOI:10.1021/jo052298n

Reference yield:

: benzyl (tert-butoxycarbonyl)oxycarbamate

: 878395-87-0
(S_S,2R,3S)-N-tert-butanesulfinyl-O-[(tert-butyloxy)carbonyl]-3-phenylisoserine

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / LiHMDS / tetrahydrofuran / -78 °C

2: 94 percent / hydrogen / Pd(OH)2 / methanol / 12 h / 760 Torr

With hydrogen; lithium hexamethyldisilazane; palladium dihydroxide; In tetrahydrofuran; methanol;
DOI:10.1021/jo052298n

Reference yield:

: 186249-74-1
(S,E)-N-benzylidene-tert-butylsulfinamide

: 878395-87-0
(S_S,2R,3S)-N-tert-butanesulfinyl-O-[(tert-butyloxy)carbonyl]-3-phenylisoserine

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / LiHMDS / tetrahydrofuran / -78 °C

2: 94 percent / hydrogen / Pd(OH)2 / methanol / 12 h / 760 Torr

With hydrogen; lithium hexamethyldisilazane; palladium dihydroxide; In tetrahydrofuran; methanol;
DOI:10.1021/jo052298n