C₃₁H₃₃N₃O₂

Base Information

Chemical Name:C₃₁H₃₃N₃O₂
CAS No.:1312938-85-4
Molecular Formula:C₃₁H₃₃N₃O₂
Molecular Weight:479.622
Hs Code.:

C<sub>31</sub>H<sub>33</sub>N<sub>3</sub>O<sub>2</sub>

Synonyms:C₃₁H₃₃N₃O₂

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Chemical Property of C₃₁H₃₃N₃O₂

Chemical Property:

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Technology Process of C₃₁H₃₃N₃O₂

There total 6 articles about C₃₁H₃₃N₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1312938-84-3
4'-[(1-benzyl-4-butyl-6-methyl-2-oxo-1,2-dihydropyridin-3-yl)methyl]biphenyl-2-carbonitrile

: 1312938-85-4
C₃₁H₃₃N₃O₂

Guidance literature:: With hydroxylamine hydrochloride; sodium hydrogencarbonate; In dimethyl sulfoxide; at 40 ℃; for 1h;

4'-[(1-benzyl-4-butyl-6-methyl-2-oxo-1,2-dihydropyridin-3-yl)methyl]biphenyl-2-carbonitrile; In dimethyl sulfoxide; at 90 ℃; for 16h;

Reference yield:

: 100-46-9
benzylamine

: 1312938-85-4
C₃₁H₃₃N₃O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: water / Reflux

2.1: N-ethyl-N,N-diisopropylamine; lithium chloride / N,N-dimethyl-formamide / 20 - 70 °C

3.1: pyridine / dichloromethane / 2 h / 20 °C

3.2: Inert atmosphere

4.1: palladium bis[bis(diphenylphosphino)ferrocene] dichloride / toluene; tetrahydrofuran / 1.5 h / 0 - 90 °C / Inert atmosphere

5.1: hydroxylamine hydrochloride; sodium hydrogencarbonate / dimethyl sulfoxide / 1 h / 40 °C

5.2: 16 h / 90 °C

With pyridine; hydroxylamine hydrochloride; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; lithium chloride; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;

Reference yield:

: 675-10-5
4-hydroxy-6-methyl-2-pyron

: 1312938-85-4
C₃₁H₃₃N₃O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: water / Reflux

2.1: N-ethyl-N,N-diisopropylamine; lithium chloride / N,N-dimethyl-formamide / 20 - 70 °C

3.1: pyridine / dichloromethane / 2 h / 20 °C

3.2: Inert atmosphere

4.1: palladium bis[bis(diphenylphosphino)ferrocene] dichloride / toluene; tetrahydrofuran / 1.5 h / 0 - 90 °C / Inert atmosphere

5.1: hydroxylamine hydrochloride; sodium hydrogencarbonate / dimethyl sulfoxide / 1 h / 40 °C

5.2: 16 h / 90 °C

With pyridine; hydroxylamine hydrochloride; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; lithium chloride; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;