(Z)-(9S,10R)-4-Benzenesulfonyl-2-((2S,5R,6R)-6-tert-butoxy-5-methyl-tetrahydro-pyran-2-yl)-10-(tert-butyl-diphenyl-silanyloxy)-9-methoxymethoxy-2-methyl-undec-6-en-3-ol

Base Information

Chemical Name:(Z)-(9S,10R)-4-Benzenesulfonyl-2-((2S,5R,6R)-6-tert-butoxy-5-methyl-tetrahydro-pyran-2-yl)-10-(tert-butyl-diphenyl-silanyloxy)-9-methoxymethoxy-2-methyl-undec-6-en-3-ol
CAS No.:86222-49-3
Molecular Formula:C₄₆H₆₈O₈SSi
Molecular Weight:809.193
Hs Code.:

(Z)-(9S,10R)-4-Benzenesulfonyl-2-((2S,5R,6R)-6-tert-butoxy-5-methyl-tetrahydro-pyran-2-yl)-10-(tert-butyl-diphenyl-silanyloxy)-9-methoxymethoxy-2-methyl-undec-6-en-3-ol

Synonyms:(Z)-(9S,10R)-4-Benzenesulfonyl-2-((2S,5R,6R)-6-tert-butoxy-5-methyl-tetrahydro-pyran-2-yl)-10-(tert-butyl-diphenyl-silanyloxy)-9-methoxymethoxy-2-methyl-undec-6-en-3-ol

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Chemical Property of (Z)-(9S,10R)-4-Benzenesulfonyl-2-((2S,5R,6R)-6-tert-butoxy-5-methyl-tetrahydro-pyran-2-yl)-10-(tert-butyl-diphenyl-silanyloxy)-9-methoxymethoxy-2-methyl-undec-6-en-3-ol

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Technology Process of (Z)-(9S,10R)-4-Benzenesulfonyl-2-((2S,5R,6R)-6-tert-butoxy-5-methyl-tetrahydro-pyran-2-yl)-10-(tert-butyl-diphenyl-silanyloxy)-9-methoxymethoxy-2-methyl-undec-6-en-3-ol

There total 8 articles about (Z)-(9S,10R)-4-Benzenesulfonyl-2-((2S,5R,6R)-6-tert-butoxy-5-methyl-tetrahydro-pyran-2-yl)-10-(tert-butyl-diphenyl-silanyloxy)-9-methoxymethoxy-2-methyl-undec-6-en-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 79698-77-4
2-((2S,5R,6R)-6-tert-Butoxy-5-methyl-tetrahydro-pyran-2-yl)-2-methyl-propionaldehyde

: 86203-38-5
((Z)-(1R,2S)-7-Benzenesulfonyl-2-methoxymethoxy-1-methyl-hept-4-enyloxy)-tert-butyl-diphenyl-silane

: 86222-49-3
(Z)-(9S,10R)-4-Benzenesulfonyl-2-((2S,5R,6R)-6-tert-butoxy-5-methyl-tetrahydro-pyran-2-yl)-10-(tert-butyl-diphenyl-silanyloxy)-9-methoxymethoxy-2-methyl-undec-6-en-3-ol

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃;

Reference yield:

: 67320-20-1,83692-41-5,94292-91-8,64722-95-8
1-(2,2-dimethyl-[1,3]dioxolan-4-yl)-3,3-bis-ethylsulfanyl-propan-1-ol

: 86222-49-3
(Z)-(9S,10R)-4-Benzenesulfonyl-2-((2S,5R,6R)-6-tert-butoxy-5-methyl-tetrahydro-pyran-2-yl)-10-(tert-butyl-diphenyl-silanyloxy)-9-methoxymethoxy-2-methyl-undec-6-en-3-ol

Guidance literature:: Multi-step reaction with 7 steps

2: 83 percent / Br₂, aqueous NaHCO₃ / diethyl ether / 5 °C

3: 75 percent / 40percent HMPA / tetrahydrofuran

4: 97 percent / 2.5percent HCl / methanol / 0 - 20 °C

5: 87 percent / Bu₃P / CH₂Cl₂ / Ambient temperature

6: 97 percent / KHSO₅ / methanol; H₂O / 0 - 20 °C

7: 95 percent / 10percent HMPA, LDA / tetrahydrofuran / -78 °C

With hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; potassium peroxomonosulfate; tributylphosphine; bromine; sodium hydrogencarbonate; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water;

Reference yield:

: 86203-37-4
(3S,4R)-4-(tert-Butyl-diphenyl-silanyloxy)-3-methoxymethoxy-pentanal

: 86222-49-3
(Z)-(9S,10R)-4-Benzenesulfonyl-2-((2S,5R,6R)-6-tert-butoxy-5-methyl-tetrahydro-pyran-2-yl)-10-(tert-butyl-diphenyl-silanyloxy)-9-methoxymethoxy-2-methyl-undec-6-en-3-ol

Guidance literature:: Multi-step reaction with 5 steps

1: 75 percent / 40percent HMPA / tetrahydrofuran

2: 97 percent / 2.5percent HCl / methanol / 0 - 20 °C

3: 87 percent / Bu₃P / CH₂Cl₂ / Ambient temperature

4: 97 percent / KHSO₅ / methanol; H₂O / 0 - 20 °C

5: 95 percent / 10percent HMPA, LDA / tetrahydrofuran / -78 °C

With hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; potassium peroxomonosulfate; tributylphosphine; lithium diisopropyl amide; In tetrahydrofuran; methanol; dichloromethane; water;