1,1,3,3-tetramethyl-1,3-bis[N-methyl-N'-(4-nitrophenylsulfonyl)propylamidomethyl]-1,3-disiloxane

Base Information

• Chemical Name: 1,1,3,3-tetramethyl-1,3-bis[N-methyl-N'-(4-nitrophenylsulfonyl)propylamidomethyl]-1,3-disiloxane
• CAS No.: 1375314-07-0
• Molecular Formula: C₃₀H₄₄N₆O₁₁S₂Si₂
• Molecular Weight: 785.016

Synonyms:1,1,3,3-tetramethyl-1,3-bis[N-methyl-N'-(4-nitrophenylsulfonyl)propylamidomethyl]-1,3-disiloxane

Chemical Property of 1,1,3,3-tetramethyl-1,3-bis[N-methyl-N'-(4-nitrophenylsulfonyl)propylamidomethyl]-1,3-disiloxane

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Technology Process of 1,1,3,3-tetramethyl-1,3-bis[N-methyl-N'-(4-nitrophenylsulfonyl)propylamidomethyl]-1,3-disiloxane

There total 1 articles about 1,1,3,3-tetramethyl-1,3-bis[N-methyl-N'-(4-nitrophenylsulfonyl)propylamidomethyl]-1,3-disiloxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

N-(dimethylchlorosilylmethyl)-N-methyl-N'-(4-nitrophenylsulfonyl)prolinamide → 1,1,3,3-tetramethyl-1,3-bis[N-methyl-N'-(4-nitrophenylsulfonyl)propylamidomethyl]-1,3-disiloxane (1375314-07-0)

Guidance literature:

With water; sodium hydrogencarbonate; In chloroform; for 24h;

DOI:10.1007/s10593-012-0949-7

Reference yield: 90.0%

1,1,3,3-tetramethyl-1,3-bis[N-methyl-N'-(4-nitrophenylsulfonyl)propylamidomethyl]-1,3-disiloxane (1375314-07-0) → N-(dimethylchlorosilylmethyl)-N-methyl-N'-(4-nitrophenylsulfonyl)prolinamide

Guidance literature:

With thionyl chloride; In benzene;

DOI:10.1007/s10593-012-0949-7

Reference yield: 90.0%

1,1,3,3-tetramethyl-1,3-bis[N-methyl-N'-(4-nitrophenylsulfonyl)propylamidomethyl]-1,3-disiloxane (1375314-07-0) → (O->Si)chelate N'-(dimethylfluorosilylmethyl)-N'-methyl-N-nosyl-(R,S)-prolinamide (1384200-34-3)

Guidance literature:

With boron trifluoride diethyl etherate; In acetonitrile; for 2h; Reflux;

DOI:10.1021/om3002697

Downstream raw materials:

(O->Si)chelate N'-(dimethylfluorosilylmethyl)-N'-methyl-N-nosyl-(R,S)-prolinamide

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