(S)-4-((4-chloro-2-((2-fluoro(¹³C₆)phenyl)sulfonyl)phenyl)sulfonyl)-alpha-methylbenzenemethanamine

Base Information

• Chemical Name: (S)-4-((4-chloro-2-((2-fluoro(¹³C₆)phenyl)sulfonyl)phenyl)sulfonyl)-alpha-methylbenzenemethanamine
• CAS No.: 1028184-26-0
• Molecular Formula: C₂₀H₁₇ClFNO₄S₂
• Molecular Weight: 459.877

Synonyms:(S)-4-((4-chloro-2-((2-fluoro(¹³C₆)phenyl)sulfonyl)phenyl)sulfonyl)-alpha-methylbenzenemethanamine

Chemical Property of (S)-4-((4-chloro-2-((2-fluoro(¹³C₆)phenyl)sulfonyl)phenyl)sulfonyl)-alpha-methylbenzenemethanamine

Chemical Property:

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Technology Process of (S)-4-((4-chloro-2-((2-fluoro(¹³C₆)phenyl)sulfonyl)phenyl)sulfonyl)-alpha-methylbenzenemethanamine

There total 4 articles about (S)-4-((4-chloro-2-((2-fluoro(¹³C₆)phenyl)sulfonyl)phenyl)sulfonyl)-alpha-methylbenzenemethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

(S)-N-(1-(4-((4-chloro-2-((2-fluoro(13C6)phenyl)sulfoxyl)phenyl)sulfonyl)phenyl)-ethyl)-2,2,2-trifluoroacetamide (1028184-23-7) → (S)-4-((4-chloro-2-((2-fluoro(13C6)phenyl)sulfonyl)phenyl)sulfonyl)-alpha-methylbenzenemethanamine (1028184-26-0)

Guidance literature:

With lithium hydroxide; In tetrahydrofuran; water; acetonitrile; for 19h;

DOI:10.1002/jlcr.1183

Reference yield:

N-{1-[4-(4-chlorobenzenesulfonyl)-phenyl]ethyl}-2,2,2-trifluoroacetamide (447460-00-6) → (S)-4-((4-chloro-2-((2-fluoro(13C6)phenyl)sulfonyl)phenyl)sulfonyl)-alpha-methylbenzenemethanamine (1028184-26-0)

Guidance literature:

Multi-step reaction with 3 steps

1: urea; hydrogen peroxide; trifluoroacetic anhydride / acetonitrile; ethyl acetate / 2.5 h / 20 °C

2: 86 percent / lithium hydroxide / acetonitrile; tetrahydrofuran; H₂O / 19 h

With lithium hydroxide; dihydrogen peroxide; urea; trifluoroacetic anhydride; In tetrahydrofuran; water; ethyl acetate; acetonitrile;

DOI:10.1002/jlcr.1183

Reference yield:

C3(13)C6H9FOS2 (1028184-51-1) → (S)-4-((4-chloro-2-((2-fluoro(13C6)phenyl)sulfonyl)phenyl)sulfonyl)-alpha-methylbenzenemethanamine (1028184-26-0)

Guidance literature:

Multi-step reaction with 3 steps

1: urea; hydrogen peroxide; trifluoroacetic anhydride / acetonitrile; ethyl acetate / 2.5 h / 20 °C

2: 86 percent / lithium hydroxide / acetonitrile; tetrahydrofuran; H₂O / 19 h

With lithium hydroxide; dihydrogen peroxide; urea; trifluoroacetic anhydride; In tetrahydrofuran; water; ethyl acetate; acetonitrile;

DOI:10.1002/jlcr.1183

upstream raw materials:

(S)-N-(1-(4-((4-chloro-2-((2-fluoro(¹³C₆)phenyl)sulfoxyl)phenyl)sulfonyl)phenyl)-ethyl)-2,2,2-trifluoroacetamide

N-{1-[4-(4-chlorobenzenesulfonyl)-phenyl]ethyl}-2,2,2-trifluoroacetamide

N-(1-{4-(4-chloro-2-(2-fluoro(¹³C)phenylsulfanyl)benzenesulfonyl)phenyl}ethyl)-2,2,2-trifluoroacetamide

C₃⁽¹³⁾C₆H₉FOS₂

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