C₅₀H₈₂O₉Si₂

Base Information

Chemical Name:C₅₀H₈₂O₉Si₂
CAS No.:1122481-19-9
Molecular Formula:C₅₀H₈₂O₉Si₂
Molecular Weight:883.367
Hs Code.:

C<sub>50</sub>H<sub>82</sub>O<sub>9</sub>Si<sub>2</sub>

Synonyms:C₅₀H₈₂O₉Si₂

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Chemical Property of C₅₀H₈₂O₉Si₂

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Technology Process of C₅₀H₈₂O₉Si₂

There total 18 articles about C₅₀H₈₂O₉Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1122481-17-7
C₄₆H₇₈O₇Si₂

: 108-24-7
acetic anhydride

: 1122481-19-9
C₅₀H₈₂O₉Si₂

Guidance literature:: With pyridine; dmap; at 0 - 20 ℃;

Reference yield: 98.0%

: C₄₆H₇₈O₇Si₂

: 108-24-7
acetic anhydride

: 1122481-19-9
C₅₀H₈₂O₉Si₂

Guidance literature:: With pyridine; dmap; at 0 ℃; for 8h; Inert atmosphere;
DOI:10.1021/ol802772s

Reference yield:

: 944393-38-8
C₃₀H₅₄O₅Si₂

: 1122481-19-9
C₅₀H₈₂O₉Si₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: n-butyllithium; potassium tert-butylate / tetrahydrofuran; hexane / 0.67 h / -78 - -46 °C

1.2: -78 °C

2.1: amberlyst resin / dichloromethane / 2 h / 20 °C

3.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / 0 - 20 °C

3.2: 5 h

4.1: sodium periodate / methanol; water / 1 h / 20 °C

5.1: boron trifluoride diethyl etherate / dichloromethane / -78 °C

6.1: benzo[1,3,2]dioxaborole / tetrahydrofuran / -78 - 0 °C

6.2: 20 °C

7.1: pyridine; dmap / 0 - 20 °C

With pyridine; dmap; sodium periodate; osmium(VIII) oxide; n-butyllithium; boron trifluoride diethyl etherate; potassium tert-butylate; 4-methylmorpholine N-oxide; benzo[1,3,2]dioxaborole; amberlyst resin; In tetrahydrofuran; methanol; hexane; dichloromethane; water; tert-butyl alcohol;