ethyl (E)-4-[4'-benzyloxy-3'-(3,5-dimethyl-1-adamantyl)phenyl]-3-chlorocinnamate

Base Information

Chemical Name:ethyl (E)-4-[4'-benzyloxy-3'-(3,5-dimethyl-1-adamantyl)phenyl]-3-chlorocinnamate
CAS No.:1063713-04-1
Molecular Formula:C₃₆H₃₉ClO₃
Molecular Weight:555.157
Hs Code.:

Synonyms:ethyl (E)-4-[4'-benzyloxy-3'-(3,5-dimethyl-1-adamantyl)phenyl]-3-chlorocinnamate

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Chemical Property of ethyl (E)-4-[4'-benzyloxy-3'-(3,5-dimethyl-1-adamantyl)phenyl]-3-chlorocinnamate

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Technology Process of ethyl (E)-4-[4'-benzyloxy-3'-(3,5-dimethyl-1-adamantyl)phenyl]-3-chlorocinnamate

There total 1 articles about ethyl (E)-4-[4'-benzyloxy-3'-(3,5-dimethyl-1-adamantyl)phenyl]-3-chlorocinnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 524937-24-4
(E)-ethyl 3-(3-chloro-4-(trifluoromethylsulphonyloxy)phenyl)acrylate

: 1063713-02-9
4-benzyloxy-3-(3,5-dimethyl-1-adamantyl)phenylboronic acid

: 1063713-04-1
ethyl (E)-4-[4'-benzyloxy-3'-(3,5-dimethyl-1-adamantyl)phenyl]-3-chlorocinnamate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; lithium chloride; In 1,2-dimethoxyethane; water; for 22h; Reflux; Inert atmosphere;
DOI:10.1021/jm800456k

Reference yield: 82.0%

: 1063713-04-1
ethyl (E)-4-[4'-benzyloxy-3'-(3,5-dimethyl-1-adamantyl)phenyl]-3-chlorocinnamate

: 1063713-07-4
ethyl (E)-3-chloro-4-[3'-(3,5-dimethyl-1-adamantyl)-4'-hydroxyphenyl]cinnamate

Guidance literature:: ethyl (E)-4-[4'-benzyloxy-3'-(3,5-dimethyl-1-adamantyl)phenyl]-3-chlorocinnamate; With phosphorus tribromide; In dichloromethane; at -78 ℃; for 2h; Inert atmosphere;

With water; In dichloromethane; for 0.25h; Inert atmosphere;
DOI:10.1021/jm800456k