Technology Process of C34H42O11
There total 11 articles about C34H42O11 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
(1S)-10-camphorsulfonic acid;
In
dichloromethane;
at 20 ℃;
for 3.5h;
Temperature;
Reagent/catalyst;
- Guidance literature:
-
With
trifluoroacetic acid;
In
toluene;
at -15 - 0 ℃;
Product distribution / selectivity;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: pyridine / dichloromethane / 27 h / 35 °C
2.1: potassium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; sodium hypochlorite solution / dichloromethane; water / 0.5 h / 0 °C
3.1: lithium aluminium tetrahydride / tetrahydrofuran; ethanol / 4 h / 0 - 10 °C / Inert atmosphere
3.2: Cooling with ice
4.1: morpholine / dichloromethane; N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere
5.1: toluene-4-sulfonic acid / methanol / 20 - 30 °C
6.1: (1S)-10-camphorsulfonic acid / dichloromethane / 3.5 h / 20 °C
With
morpholine; pyridine; lithium aluminium tetrahydride; sodium hypochlorite solution; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; (1S)-10-camphorsulfonic acid; sodium hydrogencarbonate; toluene-4-sulfonic acid; potassium bromide;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;