benzyl 2-O-n-butyl-3-(tert-butylthio)-3,4-dideoxy-α-DL-threo-pentopyranoside

Base Information

Chemical Name:benzyl 2-O-n-butyl-3-(tert-butylthio)-3,4-dideoxy-α-DL-threo-pentopyranoside
CAS No.:89017-10-7
Molecular Formula:C₂₀H₃₂O₃S
Molecular Weight:352.538
Hs Code.:

Synonyms:benzyl 2-O-n-butyl-3-(tert-butylthio)-3,4-dideoxy-α-DL-threo-pentopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 2-O-n-butyl-3-(tert-butylthio)-3,4-dideoxy-α-DL-threo-pentopyranoside

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Technology Process of benzyl 2-O-n-butyl-3-(tert-butylthio)-3,4-dideoxy-α-DL-threo-pentopyranoside

There total 3 articles about benzyl 2-O-n-butyl-3-(tert-butylthio)-3,4-dideoxy-α-DL-threo-pentopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 542-69-8
1-iodo-butane

: 89017-09-4
benzyl 3-(tert-butylthio)-3,4-dideoxy-α-DL-threo-pentopyranoside

: 89017-10-7
benzyl 2-O-n-butyl-3-(tert-butylthio)-3,4-dideoxy-α-DL-threo-pentopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1021/jo00183a016

Reference yield:

: 24923-81-7
2-benzyloxy-5,6-dihydro-α-pyran

: 89017-10-7
benzyl 2-O-n-butyl-3-(tert-butylthio)-3,4-dideoxy-α-DL-threo-pentopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 49 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 4 h

2: 1.) sodium methoxide / 1.) MeOH, 15 min 2.) reflux, 2 h

3: 90 percent / sodium hydride / dimethylformamide / Ambient temperature

With sodium methylate; sodium hydride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00183a016

Reference yield:

: 24915-72-8
benzyl 2,3-anhydro-4-deoxy-β-DL-erythro-pento-pyranoside

: 89017-10-7
benzyl 2-O-n-butyl-3-(tert-butylthio)-3,4-dideoxy-α-DL-threo-pentopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium methoxide / 1.) MeOH, 15 min 2.) reflux, 2 h

2: 90 percent / sodium hydride / dimethylformamide / Ambient temperature

With sodium methylate; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1021/jo00183a016