(1S,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)-1-(2'-pyridyl)cyclohexan-1-ol

Base Information

Chemical Name:(1S,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)-1-(2'-pyridyl)cyclohexan-1-ol
CAS No.:342898-23-1
Molecular Formula:C₂₁H₂₇NO
Molecular Weight:309.451
Hs Code.:

Synonyms:(1S,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)-1-(2'-pyridyl)cyclohexan-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)-1-(2'-pyridyl)cyclohexan-1-ol

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Technology Process of (1S,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)-1-(2'-pyridyl)cyclohexan-1-ol

There total 1 articles about (1S,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)-1-(2'-pyridyl)cyclohexan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 109-04-6
2-bromo-pyridine

: 97371-54-5
(-)-(2S,5R)-5-Methyl-2-(1-methyl-1-phenylethyl)cyclohexanon

: 342898-23-1
(1S,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)-1-(2'-pyridyl)cyclohexan-1-ol

Guidance literature:: With n-butyllithium; In diethyl ether; hexane; at 20 ℃; for 3h;
DOI:10.1016/S0022-328X(00)00774-9

Reference yield: 88.0%

: 56907-19-8,12081-12-8
bis(tetrahydrofurane)dichloridodioxidomolybdenum(VI)

: 342898-23-1
(1S,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)-1-(2'-pyridyl)cyclohexan-1-ol

: MoO₂Cl(THF)((1S,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)-1-(2'-pyridyl)cyclohexan-1-olato)

Guidance literature:: In dichloromethane; byproducts: HCl; under N2, standard Schlenk techniques; soln. of Mo complex in CH2Cl2 treated with 1 equiv. of ligand; stirred for 30 min; solvent evapd.; washed with n-hexane; dried under vac.; elem. anal.;
DOI:10.1016/S0022-328X(00)00774-9

Reference yield:

: 56907-19-8,12081-12-8
bis(tetrahydrofurane)dichloridodioxidomolybdenum(VI)

: 342898-23-1
(1S,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)-1-(2'-pyridyl)cyclohexan-1-ol

: MoO₂((1S,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)-1-(2'-pyridyl)cyclohexan-1-olato)2

Guidance literature:: In dichloromethane; byproducts: HCl; under N2, standard Schlenk techniques; soln. of Mo complex in CH2Cl2 treated with 2 equiv. of ligand; refluxed for 6 h; evapd. to dryness; washed with Et2O-n-hexane; elem. anal.;
DOI:10.1016/S0022-328X(00)00774-9