C₄₄H₄₄N₈O₆

Base Information

Chemical Name:C₄₄H₄₄N₈O₆
CAS No.:1228668-09-4
Molecular Formula:C₄₄H₄₄N₈O₆
Molecular Weight:780.883
Hs Code.:

C<sub>44</sub>H<sub>44</sub>N<sub>8</sub>O<sub>6</sub>

Synonyms:C₄₄H₄₄N₈O₆

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Chemical Property of C₄₄H₄₄N₈O₆

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Technology Process of C₄₄H₄₄N₈O₆

There total 10 articles about C₄₄H₄₄N₈O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1240428-03-8
C₃₄H₄₂N₆O₄

: 50890-96-5
(2R)-2-[(methoxycarbonyl)amino]-2-phenylacetic acid

: 1228668-09-4
C₄₄H₄₄N₈O₆

Guidance literature:: C₃₄H₄₂N₆O₄; With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 0.5h;

(2R)-2-[(methoxycarbonyl)amino]-2-phenylacetic acid; With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

Reference yield:

: 1241378-64-2
C₂₄H₂₆N₆

: 50890-96-5
(2R)-2-[(methoxycarbonyl)amino]-2-phenylacetic acid

: 1228668-09-4
C₄₄H₄₄N₈O₆

Guidance literature:: With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

Reference yield:

: 15761-39-4,59433-50-0
1-(tert-butoxycarbonyl)-L-proline

: 1228668-09-4
C₄₄H₄₄N₈O₆

Guidance literature:: Multi-step reaction with 4 steps

1.1: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 0.5 h / -20 °C

1.2: -20 - 20 °C

1.3: 2 h / 50 °C

2.1: sodium hydrogencarbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 14 h / 80 °C / Inert atmosphere

3.1: hydrogenchloride / 1,4-dioxane / 0.5 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 2 h / 20 °C

With hydrogenchloride; chloroformic acid ethyl ester; sodium hydrogencarbonate; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide;