1-cyclohexyl-2-methylenehexan-1-ol

Base Information

Chemical Name:1-cyclohexyl-2-methylenehexan-1-ol
CAS No.:871733-33-4
Molecular Formula:C₁₃H₂₄O
Molecular Weight:196.333
Hs Code.:

Synonyms:1-cyclohexyl-2-methylenehexan-1-ol

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Chemical Property of 1-cyclohexyl-2-methylenehexan-1-ol

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Technology Process of 1-cyclohexyl-2-methylenehexan-1-ol

There total 3 articles about 1-cyclohexyl-2-methylenehexan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 4426-47-5
butylboronic acid

: 1301222-91-2
2-bromo-1-cyclohexyl-2-propen-1-ol

: 871733-33-4
1-cyclohexyl-2-methylenehexan-1-ol

Guidance literature:: With dicyclohexyl(2,4,6-trimethoxyphenyl)phosphonium tetrafluoroborate; palladium diacetate; potassium carbonate; In toluene; at 110 ℃; for 3.3h; Inert atmosphere;
DOI:10.1002/ejoc.201200350

Reference yield:

: C₁₆H₃₂OSi

: 871733-33-4
1-cyclohexyl-2-methylenehexan-1-ol

Guidance literature:: With silica-gel-supported sulfuric acid; In ethyl acetate; N,N-dimethyl-formamide; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1002/chem.201500024

Reference yield:

: 54145-19-6
2-iodohex-1-ene

: 2043-61-0
cyclohexanecarbaldehyde

: 871733-33-4
1-cyclohexyl-2-methylenehexan-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1.1: (1,2-dimethoxyethane)dichloronickel(II); Mn₈₉Cr₁₁; lithium acetate; C₃₈H₄₆N₄*0.5C₄H₈O; methanol / N,N-dimethyl-formamide / 0.08 h / 20 °C / Inert atmosphere

1.2: 15 h / 20 °C / Inert atmosphere

2.1: silica-gel-supported sulfuric acid / ethyl acetate; N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

With methanol; (1,2-dimethoxyethane)dichloronickel(II); silica-gel-supported sulfuric acid; C₃₈H₄₆N₄*0.5C₄H₈O; Mn₈₉Cr₁₁; lithium acetate; In ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1002/chem.201500024