N-(benzyloxycarbonyl)-O-(N-Boc-L-valyl)-D-serine p-chlorophenacyl ester

Base Information

Chemical Name:N-(benzyloxycarbonyl)-O-(N-Boc-L-valyl)-D-serine p-chlorophenacyl ester
CAS No.:103131-29-9
Molecular Formula:C₂₉H₃₅ClN₂O₉
Molecular Weight:591.058
Hs Code.:

Synonyms:N-(benzyloxycarbonyl)-O-(N-Boc-L-valyl)-D-serine p-chlorophenacyl ester

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Chemical Property of N-(benzyloxycarbonyl)-O-(N-Boc-L-valyl)-D-serine p-chlorophenacyl ester

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Technology Process of N-(benzyloxycarbonyl)-O-(N-Boc-L-valyl)-D-serine p-chlorophenacyl ester

There total 3 articles about N-(benzyloxycarbonyl)-O-(N-Boc-L-valyl)-D-serine p-chlorophenacyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 13734-41-3
t-Boc-L-valine

: 103131-28-8
N-(benzyloxycarbonyl)-D-serine p-chlorophenacyl ester

: 103131-29-9
N-(benzyloxycarbonyl)-O-(N-Boc-L-valyl)-D-serine p-chlorophenacyl ester

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In pyridine; at 0 - 20 ℃; for 24h;
DOI:10.1021/jo00366a001

Reference yield:

: 6081-61-4
N-(benzyloxycarbonyl)-D-serine

: 103131-29-9
N-(benzyloxycarbonyl)-O-(N-Boc-L-valyl)-D-serine p-chlorophenacyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / K₂CO₃ / acetone / 7 h / Heating

2: 81 percent / HOBt, DCC / pyridine / 24 h / 0 - 20 °C

With potassium carbonate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In pyridine; acetone;
DOI:10.1021/jo00366a001

Reference yield:

: 536-38-9
4-chlorobenzoylmethyl bromide

: 103131-29-9
N-(benzyloxycarbonyl)-O-(N-Boc-L-valyl)-D-serine p-chlorophenacyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / K₂CO₃ / acetone / 7 h / Heating

2: 81 percent / HOBt, DCC / pyridine / 24 h / 0 - 20 °C

With potassium carbonate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In pyridine; acetone;
DOI:10.1021/jo00366a001