[closo-3,3-(PMe₂Ph)2-3-Cl-3,1,2-RhC₂B₉H₁₁]

Base Information

Chemical Name:[closo-3,3-(PMe₂Ph)2-3-Cl-3,1,2-RhC₂B₉H₁₁]
CAS No.:89363-55-3
Molecular Formula:C₁₈H₃₃B₉ClP₂Rh
Molecular Weight:547.065
Hs Code.:

[closo-3,3-(PMe<sub>2</sub>Ph)2-3-Cl-3,1,2-RhC<sub>2</sub>B<sub>9</sub>H<sub>11</sub>]

Synonyms:[closo-3,3-(PMe₂Ph)2-3-Cl-3,1,2-RhC₂B₉H₁₁]

Suppliers and Price of [closo-3,3-(PMe₂Ph)2-3-Cl-3,1,2-RhC₂B₉H₁₁]

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Chemical Property of [closo-3,3-(PMe₂Ph)2-3-Cl-3,1,2-RhC₂B₉H₁₁]

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Technology Process of [closo-3,3-(PMe₂Ph)2-3-Cl-3,1,2-RhC₂B₉H₁₁]

There total 3 articles about [closo-3,3-(PMe₂Ph)2-3-Cl-3,1,2-RhC₂B₉H₁₁] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 89363-53-1
[closo-3,3-(PMe₂Ph)2-3-H-3,1,2-RhC₂B₉H₁₁]

: 89363-55-3
[closo-3,3-(PMe₂Ph)2-3-Cl-3,1,2-RhC₂B₉H₁₁]

Guidance literature:: With CH₂Cl₂; In dichloromethane; Rh complex dissolved in CH2Cl2, stirred for 12 h; layered with heptane; elem. anal.;
DOI:10.1021/ja00322a038

Reference yield: 95.0%

: 82808-03-5
[closo-3,3-(dimethylphenylphosphine)2-3-NO₃-3,1,2-RhC₂B₉H₁₁]

: 89363-55-3
[closo-3,3-(PMe₂Ph)2-3-Cl-3,1,2-RhC₂B₉H₁₁]

Guidance literature:: With HCl; In tetrahydrofuran; under Ar, 37% HCl added to THF soln. of Rh complex, mixt. stirred for 15 min at room temp., further drops of HCl added, stirred for 75 min; heptane added, THF removed in vac., ppt. filtered off in air, washed with pentane, dried by suction;