C₄₃H₅₈O₁₁Si

Base Information

Chemical Name:C₄₃H₅₈O₁₁Si
CAS No.:153145-51-8
Molecular Formula:C₄₃H₅₈O₁₁Si
Molecular Weight:779.012
Hs Code.:

C<sub>43</sub>H<sub>58</sub>O<sub>11</sub>Si

Synonyms:C₄₃H₅₈O₁₁Si

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Chemical Property of C₄₃H₅₈O₁₁Si

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Technology Process of C₄₃H₅₈O₁₁Si

There total 23 articles about C₄₃H₅₈O₁₁Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 153145-26-7
C₃₂H₅₆O₇Si₂

C₄₃H₅₈O₁₁Si: 153145-51-8
C₄₃H₅₈O₁₁Si

Guidance literature:: Multi-step reaction with 12 steps

1: 92 percent / EtN(i-Pr)2, (Bu)4NI / CH₂Cl₂ / 32 h / Heating

2: 1.) LDA, 2.) mCPBA / 1.) THF, -78 deg C, 2.) hexane, 25 deg C, 5 h

3: 95 percent / CH₂Cl₂ / 15 h / -45 °C

4: 63 percent / Burgess' reagent

5: 100 percent / pyridine

6: 65 percent / OsO₄

7: DBU / toluene / 2 h / 105 °C

8: 75 percent / pyridine, DMAP / 24 h / 25 °C

9: 100 percent / HF*pyridine / acetonitrile / 11 h / 0 °C

10: tetrahydrofuran / 0.17 h / -78 °C

11: tetrapropylammonium perruthenate, NMO, molecular sieves / CH₂Cl₂ / 0.25 h / 25 °C

12: 1.) t-BuOK, 2.) benzeneseleninic anhydride, 3.) t-BuOK

With pyridine; dmap; osmium(VIII) oxide; N-methyl-2-indolinone; molecular sieve; tetrapropylammonium perruthennate; Burgess Reagent; benzeneseleninic anhydride; potassium tert-butylate; tetra-(n-butyl)ammonium iodide; pyridine hydrogenfluoride; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; toluene; acetonitrile;

Reference yield:

: 153145-56-3
C₃₃H₅₆O₈Si₂

C₄₃H₅₈O₁₁Si: 153145-51-8
C₄₃H₅₈O₁₁Si

Guidance literature:: Multi-step reaction with 18 steps

1: KMnO₄, KH₂PO₄

3: 93 percent / LDA / tetrahydrofuran / 0.5 h / -78 °C

4: 100 percent / p-TsOH

5: 92 percent / PhSK / dimethylformamide / 3 h / 86 °C

6: acid

7: 92 percent / EtN(i-Pr)2, (Bu)4NI / CH₂Cl₂ / 32 h / Heating

8: 1.) LDA, 2.) mCPBA / 1.) THF, -78 deg C, 2.) hexane, 25 deg C, 5 h

9: 95 percent / CH₂Cl₂ / 15 h / -45 °C

10: 63 percent / Burgess' reagent

11: 100 percent / pyridine

12: 65 percent / OsO₄

13: DBU / toluene / 2 h / 105 °C

14: 75 percent / pyridine, DMAP / 24 h / 25 °C

15: 100 percent / HF*pyridine / acetonitrile / 11 h / 0 °C

16: tetrahydrofuran / 0.17 h / -78 °C

17: tetrapropylammonium perruthenate, NMO, molecular sieves / CH₂Cl₂ / 0.25 h / 25 °C

18: 1.) t-BuOK, 2.) benzeneseleninic anhydride, 3.) t-BuOK

With pyridine; dmap; potassium permanganate; potassium dihydrogenphosphate; osmium(VIII) oxide; N-methyl-2-indolinone; molecular sieve; tetrapropylammonium perruthennate; Burgess Reagent; benzeneseleninic anhydride; potassium tert-butylate; tetra-(n-butyl)ammonium iodide; (2E)-3-(4-hydroxyphenyl-3-methoxyphenyl)-1-phenylprop-2-en-1-one; toluene-4-sulfonic acid; pyridine hydrogenfluoride; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 153145-20-1
C₃₄H₅₈O₇Si₂

C₄₃H₅₈O₁₁Si: 153145-51-8
C₄₃H₅₈O₁₁Si

Guidance literature:: Multi-step reaction with 19 steps

1: O₃

2: KMnO₄, KH₂PO₄

4: 93 percent / LDA / tetrahydrofuran / 0.5 h / -78 °C

5: 100 percent / p-TsOH

6: 92 percent / PhSK / dimethylformamide / 3 h / 86 °C

7: acid

8: 92 percent / EtN(i-Pr)2, (Bu)4NI / CH₂Cl₂ / 32 h / Heating

9: 1.) LDA, 2.) mCPBA / 1.) THF, -78 deg C, 2.) hexane, 25 deg C, 5 h

10: 95 percent / CH₂Cl₂ / 15 h / -45 °C

11: 63 percent / Burgess' reagent

12: 100 percent / pyridine

13: 65 percent / OsO₄

14: DBU / toluene / 2 h / 105 °C

15: 75 percent / pyridine, DMAP / 24 h / 25 °C

16: 100 percent / HF*pyridine / acetonitrile / 11 h / 0 °C

17: tetrahydrofuran / 0.17 h / -78 °C

18: tetrapropylammonium perruthenate, NMO, molecular sieves / CH₂Cl₂ / 0.25 h / 25 °C

19: 1.) t-BuOK, 2.) benzeneseleninic anhydride, 3.) t-BuOK

With pyridine; dmap; potassium permanganate; potassium dihydrogenphosphate; osmium(VIII) oxide; N-methyl-2-indolinone; molecular sieve; tetrapropylammonium perruthennate; Burgess Reagent; benzeneseleninic anhydride; potassium tert-butylate; tetra-(n-butyl)ammonium iodide; (2E)-3-(4-hydroxyphenyl-3-methoxyphenyl)-1-phenylprop-2-en-1-one; toluene-4-sulfonic acid; pyridine hydrogenfluoride; ozone; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;