1-{4-[α-(1-tricyclo[3.3.1.1^3,7]decyl)phenylmethyl]phenylcarbonyl}pireridine

Base Information

Chemical Name:1-{4-[α-(1-tricyclo[3.3.1.1^3,7]decyl)phenylmethyl]phenylcarbonyl}pireridine
CAS No.:1410789-56-8
Molecular Formula:C₂₉H₃₅NO
Molecular Weight:413.603
Hs Code.:

1-{4-[α-(1-tricyclo[3.3.1.1<sup>3,7</sup>]decyl)phenylmethyl]phenylcarbonyl}pireridine

Synonyms:1-{4-[α-(1-tricyclo[3.3.1.1^3,7]decyl)phenylmethyl]phenylcarbonyl}pireridine

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Chemical Property of 1-{4-[α-(1-tricyclo[3.3.1.1^3,7]decyl)phenylmethyl]phenylcarbonyl}pireridine

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Technology Process of 1-{4-[α-(1-tricyclo[3.3.1.1^3,7]decyl)phenylmethyl]phenylcarbonyl}pireridine

There total 5 articles about 1-{4-[α-(1-tricyclo[3.3.1.1^3,7]decyl)phenylmethyl]phenylcarbonyl}pireridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1410789-54-6
4-bromo-α-phenyl-α-(1-tricyclo[3.3.1.1^3,7]decyl)methylbenzene

: 1410789-56-8
1-{4-[α-(1-tricyclo[3.3.1.1^3,7]decyl)phenylmethyl]phenylcarbonyl}pireridine

Guidance literature:: Multi-step reaction with 3 steps

1.1: magnesium; iodine / tetrahydrofuran; ethylene dibromide / 3 h / Inert atmosphere; Reflux

1.2: 3 h / 20 °C / Inert atmosphere

1.3: 0 °C / Inert atmosphere

2.1: thionyl chloride / 1 h / Reflux

3.1: tetrahydrofuran / 3 h / 0 °C / Reflux

With thionyl chloride; iodine; magnesium; In tetrahydrofuran; ethylene dibromide;
DOI:10.1021/jm3013008

Reference yield:

: 4-[α-(1-tricyclo[3.3.1.1^3,7]decyl)phenylmethyl]benzene carboxylic acid

: 1410789-56-8
1-{4-[α-(1-tricyclo[3.3.1.1^3,7]decyl)phenylmethyl]phenylcarbonyl}pireridine

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 1 h / Reflux

2: tetrahydrofuran / 3 h / 0 °C / Reflux

With thionyl chloride; In tetrahydrofuran;
DOI:10.1021/jm3013008

Reference yield:

: 106-37-6
1.4-dibromobenzene

: 1410789-56-8
1-{4-[α-(1-tricyclo[3.3.1.1^3,7]decyl)phenylmethyl]phenylcarbonyl}pireridine

Guidance literature:: Multi-step reaction with 5 steps

1.1: magnesium / diethyl ether / Inert atmosphere; Reflux

1.2: 0 °C / Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane / 0.25 h / 20 °C / Inert atmosphere

2.2: 1 h / 20 °C / Inert atmosphere

2.3: 0 °C

3.1: magnesium; iodine / tetrahydrofuran; ethylene dibromide / 3 h / Inert atmosphere; Reflux

3.2: 3 h / 20 °C / Inert atmosphere

3.3: 0 °C / Inert atmosphere

4.1: thionyl chloride / 1 h / Reflux

5.1: tetrahydrofuran / 3 h / 0 °C / Reflux

With thionyl chloride; iodine; magnesium; trifluoroacetic acid; In tetrahydrofuran; diethyl ether; dichloromethane; ethylene dibromide;
DOI:10.1021/jm3013008