4-(2-(2-(allyloxy)-4-(bis(2-hydroxyethyl)amino)phenyl)-2H-tetrazol-5-yl)benzaldehyde

Base Information

Chemical Name:4-(2-(2-(allyloxy)-4-(bis(2-hydroxyethyl)amino)phenyl)-2H-tetrazol-5-yl)benzaldehyde
CAS No.:1315336-63-0
Molecular Formula:C₂₁H₂₃N₅O₄
Molecular Weight:409.445
Hs Code.:

Synonyms:4-(2-(2-(allyloxy)-4-(bis(2-hydroxyethyl)amino)phenyl)-2H-tetrazol-5-yl)benzaldehyde

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Chemical Property of 4-(2-(2-(allyloxy)-4-(bis(2-hydroxyethyl)amino)phenyl)-2H-tetrazol-5-yl)benzaldehyde

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Technology Process of 4-(2-(2-(allyloxy)-4-(bis(2-hydroxyethyl)amino)phenyl)-2H-tetrazol-5-yl)benzaldehyde

There total 7 articles about 4-(2-(2-(allyloxy)-4-(bis(2-hydroxyethyl)amino)phenyl)-2H-tetrazol-5-yl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1315336-62-9
4-(2-(2-(allyloxy)-4-(bis(2-((tert-butyldimethylsilyl)oxy)ethyl)amino)phenyl)-2H-tetrazol-5-yl) benzaldehyde

: 1315336-63-0
4-(2-(2-(allyloxy)-4-(bis(2-hydroxyethyl)amino)phenyl)-2H-tetrazol-5-yl)benzaldehyde

Guidance literature:: With water; acetic acid; trifluoroacetic acid; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1021/ja204758c

Reference yield:

: 1315336-57-2
methyl 4-(2-(2-(allyloxy)-4-nitrophenyl)-2H-tetrazol-5-yl)benzoate

: 1315336-63-0
4-(2-(2-(allyloxy)-4-(bis(2-hydroxyethyl)amino)phenyl)-2H-tetrazol-5-yl)benzaldehyde

Guidance literature:: Multi-step reaction with 6 steps

1: ethanol; water; iron; acetic acid / Sonication

2: methanol / dichloromethane / 15 h / -78 - 70 °C / pressurized reaction vessel

3: 1H-imidazole; triethylamine / dichloromethane; N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

4: lithium aluminium tetrahydride / tetrahydrofuran / 0.01 h / 0 °C / Inert atmosphere

5: Dess-Martin periodane / dichloromethane / 2 h / 20 °C

6: water; acetic acid; trifluoroacetic acid / dichloromethane / 2 h / 0 °C

With 1H-imidazole; methanol; lithium aluminium tetrahydride; ethanol; water; iron; Dess-Martin periodane; acetic acid; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja204758c

Reference yield:

: 351188-76-6
(E)-methyl 4-((2-(phenylsulfonyl)hydrazono)methyl)benzoate

: 1315336-63-0
4-(2-(2-(allyloxy)-4-(bis(2-hydroxyethyl)amino)phenyl)-2H-tetrazol-5-yl)benzaldehyde

Guidance literature:: Multi-step reaction with 7 steps

1: pyridine / -20 °C

2: ethanol; water; iron; acetic acid / Sonication

3: methanol / dichloromethane / 15 h / -78 - 70 °C / pressurized reaction vessel

4: 1H-imidazole; triethylamine / dichloromethane; N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

5: lithium aluminium tetrahydride / tetrahydrofuran / 0.01 h / 0 °C / Inert atmosphere

6: Dess-Martin periodane / dichloromethane / 2 h / 20 °C

7: water; acetic acid; trifluoroacetic acid / dichloromethane / 2 h / 0 °C

With pyridine; 1H-imidazole; methanol; lithium aluminium tetrahydride; ethanol; water; iron; Dess-Martin periodane; acetic acid; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja204758c