2-[4-(3-chloropropoxy)phenyl]-N-(cyclopropylmethyl)-4-methyl-N-propyl-1,3-oxazole-5-carboxamide

Base Information

Chemical Name:2-[4-(3-chloropropoxy)phenyl]-N-(cyclopropylmethyl)-4-methyl-N-propyl-1,3-oxazole-5-carboxamide
CAS No.:911134-85-5
Molecular Formula:C₂₁H₂₇ClN₂O₃
Molecular Weight:390.91
Hs Code.:

Synonyms:2-[4-(3-chloropropoxy)phenyl]-N-(cyclopropylmethyl)-4-methyl-N-propyl-1,3-oxazole-5-carboxamide

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Chemical Property of 2-[4-(3-chloropropoxy)phenyl]-N-(cyclopropylmethyl)-4-methyl-N-propyl-1,3-oxazole-5-carboxamide

Chemical Property:

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Technology Process of 2-[4-(3-chloropropoxy)phenyl]-N-(cyclopropylmethyl)-4-methyl-N-propyl-1,3-oxazole-5-carboxamide

There total 5 articles about 2-[4-(3-chloropropoxy)phenyl]-N-(cyclopropylmethyl)-4-methyl-N-propyl-1,3-oxazole-5-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₄H₁₃Cl₂NO₃

: 26389-60-6
N-(n-propyl)-N-(cyclopropanemethyl)amine

: 911134-85-5
2-[4-(3-chloropropoxy)phenyl]-N-(cyclopropylmethyl)-4-methyl-N-propyl-1,3-oxazole-5-carboxamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 619-57-8
p-hydroxybenzamide

: 911134-85-5
2-[4-(3-chloropropoxy)phenyl]-N-(cyclopropylmethyl)-4-methyl-N-propyl-1,3-oxazole-5-carboxamide

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / butanone / 48 h / Heating / reflux

2: ethanol / 24 h / 110 °C

3: methanol; sodium hydroxide; water / 2 h / 60 °C

4: thionyl chloride; triethylamine / chloroform / 2.5 h / Heating / reflux

5: triethylamine / dichloromethane / 0 - 20 °C

With methanol; sodium hydroxide; thionyl chloride; water; potassium carbonate; triethylamine; In ethanol; dichloromethane; chloroform; butanone;

Reference yield:

: 911134-52-6
methyl 2-[4-(3-chloropropoxy)phenyl]-4-methyl-1,3-oxazole-5-carboxylate

: 911134-85-5
2-[4-(3-chloropropoxy)phenyl]-N-(cyclopropylmethyl)-4-methyl-N-propyl-1,3-oxazole-5-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: methanol; sodium hydroxide; water / 2 h / 60 °C

2: thionyl chloride; triethylamine / chloroform / 2.5 h / Heating / reflux

3: triethylamine / dichloromethane / 0 - 20 °C

With methanol; sodium hydroxide; thionyl chloride; water; triethylamine; In dichloromethane; chloroform;