anti-9-diphenylphosphoryl-5,5-dimethyl-3,4,11,12-tetraza-exo,endo-tetracyclo<5.3.2.0^2,6.0^8,10>dodec-3-ene-11,12-dicarboxylic acid phenylimide

Base Information

• Chemical Name: anti-9-diphenylphosphoryl-5,5-dimethyl-3,4,11,12-tetraza-exo,endo-tetracyclo<5.3.2.0^2,6.0^8,10>dodec-3-ene-11,12-dicarboxylic acid phenylimide
• CAS No.: 90652-62-3
• Molecular Formula: C₃₀H₂₈N₅O₃P
• Molecular Weight: 537.558

Synonyms:anti-9-diphenylphosphoryl-5,5-dimethyl-3,4,11,12-tetraza-exo,endo-tetracyclo<5.3.2.0^2,6.0^8,10>dodec-3-ene-11,12-dicarboxylic acid phenylimide

Chemical Property of anti-9-diphenylphosphoryl-5,5-dimethyl-3,4,11,12-tetraza-exo,endo-tetracyclo<5.3.2.0^2,6.0^8,10>dodec-3-ene-11,12-dicarboxylic acid phenylimide

Chemical Property:

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Technology Process of anti-9-diphenylphosphoryl-5,5-dimethyl-3,4,11,12-tetraza-exo,endo-tetracyclo<5.3.2.0^2,6.0^8,10>dodec-3-ene-11,12-dicarboxylic acid phenylimide

There total 1 articles about anti-9-diphenylphosphoryl-5,5-dimethyl-3,4,11,12-tetraza-exo,endo-tetracyclo<5.3.2.0^2,6.0^8,10>dodec-3-ene-11,12-dicarboxylic acid phenylimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

anti-3-Diphenylphosphoryl-6,7-diaza-exo-tricyclo<3.2.2.02,4>non-8-en-6,7-dicarbonsaeure-phenylimid (81268-09-9) + 2-diazopropane (2684-60-8) → anti-9-diphenylphosphoryl-5,5-dimethyl-3,4,11,12-tetraza-exo,endo-tetracyclo<5.3.2.02,6.08,10>dodec-3-ene-11,12-dicarboxylic acid phenylimide (90652-62-3)

Guidance literature:

In diethyl ether; N,N-dimethyl-formamide; at -15 ℃; for 10h;

DOI:10.1016/S0040-4020(01)91187-1

Reference yield: 68.0%

anti-9-diphenylphosphoryl-5,5-dimethyl-3,4,11,12-tetraza-exo,endo-tetracyclo<5.3.2.02,6.08,10>dodec-3-ene-11,12-dicarboxylic acid phenylimide (90652-62-3) → anti-3-diphenylphosphoryl-7,7-dimethyl-9,10-diaza-endo,exo-tetracyclo<3.3.2.02,4.06,8>decane-9,10-dicarboxylic acid phenylimide (90652-81-6)

Guidance literature:

In acetonitrile; Ambient temperature; Irradiation;

DOI:10.1016/S0040-4020(01)91187-1

Reference yield:

anti-9-diphenylphosphoryl-5,5-dimethyl-3,4,11,12-tetraza-exo,endo-tetracyclo<5.3.2.02,6.08,10>dodec-3-ene-11,12-dicarboxylic acid phenylimide (90652-62-3) → C22H23N2OP*ClCu

Guidance literature:

Multi-step reaction with 2 steps

1: 68 percent / acetonitrile / Ambient temperature; Irradiation

2: 1.) NaOH 2.) 1 N HCl, CuCl₂*2H₂O / 1.) 2-propanol, reflux, 70 min 2.) water, 0 deg C; then room temp., 1 h

With hydrogenchloride; sodium hydroxide; In acetonitrile;

DOI:10.1016/S0040-4020(01)91187-1

upstream raw materials:

anti-3-Diphenylphosphoryl-6,7-diaza-exo-tricyclo<3.2.2.0^2,4>non-8-en-6,7-dicarbonsaeure-phenylimid

2-diazopropane

Downstream raw materials:

anti-3-diphenylphosphoryl-7,7-dimethyl-9,10-diaza-endo,exo-tetracyclo<3.3.2.0^2,4.0^6,8>decane-9,10-dicarboxylic acid phenylimide

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