benzyl (bis(4-(methylthio)phenoxy)phosphoryl)(4-nitrophenyl)methylcarbamate

Base Information

Chemical Name:benzyl (bis(4-(methylthio)phenoxy)phosphoryl)(4-nitrophenyl)methylcarbamate
CAS No.:890136-21-7
Molecular Formula:C₂₉H₂₇N₂O₇PS₂
Molecular Weight:610.648
Hs Code.:

Synonyms:benzyl (bis(4-(methylthio)phenoxy)phosphoryl)(4-nitrophenyl)methylcarbamate

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Chemical Property of benzyl (bis(4-(methylthio)phenoxy)phosphoryl)(4-nitrophenyl)methylcarbamate

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Technology Process of benzyl (bis(4-(methylthio)phenoxy)phosphoryl)(4-nitrophenyl)methylcarbamate

There total 1 articles about benzyl (bis(4-(methylthio)phenoxy)phosphoryl)(4-nitrophenyl)methylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 22945-49-9
tris(4-(methylthio)phenyl) phosphite

: 621-84-1
O-benzyl carbamate

: 555-16-8
4-nitrobenzaldehdye

: 890136-21-7
benzyl (bis(4-(methylthio)phenoxy)phosphoryl)(4-nitrophenyl)methylcarbamate

Guidance literature:: With acetic acid; at 90 ℃; for 3h;
DOI:10.1016/j.bmcl.2006.03.002

Reference yield: 88.0%

: 890136-21-7
benzyl (bis(4-(methylthio)phenoxy)phosphoryl)(4-nitrophenyl)methylcarbamate

: C₂₉H₂₉N₂O₅PS₂

Guidance literature:: With tin(ll) chloride; In ethyl acetate; for 12h; Heating;
DOI:10.1016/j.bmcl.2006.03.002

Reference yield:

: 890136-21-7
benzyl (bis(4-(methylthio)phenoxy)phosphoryl)(4-nitrophenyl)methylcarbamate

: (S)-bis(4-(methylthio)phenyl) (2-(4-nitrobenzamido)-3-phenylpropanamido)(4-nitrophenyl)methylphosphonate

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid; hydrogen bromide / 0.5 h / 20 °C

2: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

3: dichloromethane / 1 h / 20 °C

4: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

With hydrogen bromide; acetic acid; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.201600206