C₃₄H₃₀N₈O₆S₂

Base Information

• Chemical Name: C₃₄H₃₀N₈O₆S₂
• CAS No.: 890085-24-2
• Molecular Formula: C₃₄H₃₀N₈O₆S₂
• Molecular Weight: 710.794

Synonyms:C₃₄H₃₀N₈O₆S₂

Chemical Property of C₃₄H₃₀N₈O₆S₂

Chemical Property:

Purity/Quality:

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Technology Process of C₃₄H₃₀N₈O₆S₂

There total 25 articles about C₃₄H₃₀N₈O₆S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C34H32N8O6S2 → C34H30N8O6S2 (890085-24-2) + C34H30N8O6S2 (1445860-29-6)

Guidance literature:

With Bromotrichloromethane; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at -78 - 20 ℃; Overall yield = 1.5 mg; Inert atmosphere;

DOI:10.1021/ol401412v

Reference yield:

C35H34N8O9S3 → C34H30N8O6S2 (890085-24-2)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃; for 1.5h; Inert atmosphere;

DOI:10.1002/ejoc.201600994

Reference yield:

(S)-2-(1’-((tert-butoxycarbonyl)amino)-2’-(tritylthio)ethyl)thiazole-4-carboxylic acid methyl ester → C34H30N8O6S2 (890085-24-2)

Guidance literature:

Multi-step reaction with 14 steps

1.1: hydrogenchloride / 1,4-dioxane / 20 h / 20 °C / Inert atmosphere

2.1: triethylamine; triflic azide; zinc(II) sulfate / water; dichloromethane; methanol / 2.5 h / 0 - 20 °C / Inert atmosphere

3.1: sodium hydroxide / water; dichloromethane; methanol; 2,2,2-trifluoroethanol / 72 h / 0 - 20 °C / Inert atmosphere

4.1: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide; dichloromethane / 3.5 h / 0 - 20 °C / Inert atmosphere

5.1: (bis-(2-methoxyethyl)amino)sulfur trufluoride / tetrahydrofuran / 3 h / -65 °C / Inert atmosphere

5.2: 1 h / -60 - 20 °C / Inert atmosphere

6.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.33 h / -50 °C / Inert atmosphere

6.2: 29 h / -25 °C / Inert atmosphere

7.1: trimethyltin(IV) hydroxide / 1,2-dichloro-ethane / 80 °C / Inert atmosphere

8.1: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dichloromethane / 0.42 h / 0 °C / Inert atmosphere

8.2: 48 h / 20 °C / Inert atmosphere

9.1: bis(dibenzylideneacetone)-palladium⁽⁰⁾; morpholine / dichloromethane / 4 h / 20 °C / Inert atmosphere

10.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / N,N-dimethyl-formamide; dichloromethane / 24 h / 20 °C / Inert atmosphere

11.1: triphenylphosphine; 2,6-dimethylpyridine / 7 h / 60 °C / Inert atmosphere

12.1: 1,8-diazabicyclo[5.4.0]undec-7-ene; Bromotrichloromethane / dichloromethane / 8 h / -70 - 20 °C / Inert atmosphere

13.1: triethylamine; 2,6-dimethylpyridine / dichloromethane / 2.5 h / 20 °C / Inert atmosphere

14.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

With morpholine; 2,6-dimethylpyridine; hydrogenchloride; Bromotrichloromethane; triflic azide; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; zinc(II) sulfate; trimethyltin(IV) hydroxide; sodium hydroxide; (bis-(2-methoxyethyl)amino)sulfur trufluoride; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; 2,2,2-trifluoroethanol; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

DOI:10.1002/ejoc.201600994

upstream raw materials:

(2R,1'S)-(1’-((tert-butoxycarbonyl)amino)-2’-(tritylthio)ethyl)-4,5-dihydrothiazole-4-carboxylic acid methyl ester

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