1-(1H-benzotriazol-1-yl)-2-chloro-1-[(3,4-dichlorophenyl)imino]-2-nitroethane

Base Information

• Chemical Name: 1-(1H-benzotriazol-1-yl)-2-chloro-1-[(3,4-dichlorophenyl)imino]-2-nitroethane
• CAS No.: 1374634-41-9
• Molecular Formula: C₁₄H₈Cl₃N₅O₂
• Molecular Weight: 384.609

Synonyms:1-(1H-benzotriazol-1-yl)-2-chloro-1-[(3,4-dichlorophenyl)imino]-2-nitroethane

Chemical Property of 1-(1H-benzotriazol-1-yl)-2-chloro-1-[(3,4-dichlorophenyl)imino]-2-nitroethane

Chemical Property:

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Technology Process of 1-(1H-benzotriazol-1-yl)-2-chloro-1-[(3,4-dichlorophenyl)imino]-2-nitroethane

There total 2 articles about 1-(1H-benzotriazol-1-yl)-2-chloro-1-[(3,4-dichlorophenyl)imino]-2-nitroethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

1,1-bis(1H-benzotriazol-1-yl)-2-chloro-2-nitroethene (350024-43-0) + m,p-dichloroaniline (95-76-1) → 1-(1H-benzotriazol-1-yl)-2-chloro-1-[(3,4-dichlorophenyl)imino]-2-nitroethane (1374634-41-9)

Guidance literature:

In methanol; at 20 - 40 ℃; for 7h;

DOI:10.1055/s-0031-1289716

Reference yield:

1,2,3-Benzotriazole (95-14-7,27556-51-0) → 1-(1H-benzotriazol-1-yl)-2-chloro-1-[(3,4-dichlorophenyl)imino]-2-nitroethane (1374634-41-9)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran / 50 h / 20 °C / Reflux

2: methanol / 7 h / 20 - 40 °C

In tetrahydrofuran; methanol;

DOI:10.1055/s-0031-1289716

Reference yield: 77.0%

1-(1H-benzotriazol-1-yl)-2-chloro-1-[(3,4-dichlorophenyl)imino]-2-nitroethane (1374634-41-9) → 5-[chloro(nitro)methyl]-1-(3,4-dichlorophenyl)-1H-tetrazole (1374634-48-6)

Guidance literature:

With sodium azide; In methanol; at -5 - 20 ℃; for 8h;

DOI:10.1055/s-0031-1289716

upstream raw materials:

1,2,3-Benzotriazole

1,1-bis(1H-benzotriazol-1-yl)-2-chloro-2-nitroethene

m,p-dichloroaniline

Downstream raw materials:

5-[chloro(nitro)methyl]-1-(3,4-dichlorophenyl)-1H-tetrazole

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