(3R,7R,10S)-10-[(tert-butyldiphenyl)silyl]oxy-7-hydroxy-3-methyl-5-methyleneundec-1-ene

Base Information

Chemical Name:(3R,7R,10S)-10-[(tert-butyldiphenyl)silyl]oxy-7-hydroxy-3-methyl-5-methyleneundec-1-ene
CAS No.:1259928-75-0
Molecular Formula:C₂₉H₄₂O₂Si
Molecular Weight:450.737
Hs Code.:

Synonyms:(3R,7R,10S)-10-[(tert-butyldiphenyl)silyl]oxy-7-hydroxy-3-methyl-5-methyleneundec-1-ene

Suppliers and Price of (3R,7R,10S)-10-[(tert-butyldiphenyl)silyl]oxy-7-hydroxy-3-methyl-5-methyleneundec-1-ene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3R,7R,10S)-10-[(tert-butyldiphenyl)silyl]oxy-7-hydroxy-3-methyl-5-methyleneundec-1-ene

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Technology Process of (3R,7R,10S)-10-[(tert-butyldiphenyl)silyl]oxy-7-hydroxy-3-methyl-5-methyleneundec-1-ene

There total 2 articles about (3R,7R,10S)-10-[(tert-butyldiphenyl)silyl]oxy-7-hydroxy-3-methyl-5-methyleneundec-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1259928-80-7
(3R,7R,10S)-10-[(tert-butyldiphenyl)silyl]oxy-3-methyl-5-methylene-7-(triethylsilyl)oxyundec-1-ene

: 1259928-75-0
(3R,7R,10S)-10-[(tert-butyldiphenyl)silyl]oxy-7-hydroxy-3-methyl-5-methyleneundec-1-ene

Guidance literature:: With trifluoroacetic acid; In tetrahydrofuran; water; at 20 ℃; for 2.5h;
DOI:10.1002/chem.201001794

Reference yield: 16.0%

: nysted reagent

: 1259928-79-4
(3R,7R,10S)-10-[(tert-butyldiphenyl)silyl]oxy-3-methyl-7-(triethylsilyl)oxyundec-1-en-5-one

: 1259928-75-0
(3R,7R,10S)-10-[(tert-butyldiphenyl)silyl]oxy-7-hydroxy-3-methyl-5-methyleneundec-1-ene

: 1259928-80-7
(3R,7R,10S)-10-[(tert-butyldiphenyl)silyl]oxy-3-methyl-5-methylene-7-(triethylsilyl)oxyundec-1-ene

Guidance literature:: With titanium tetrachloride; In tetrahydrofuran; for 1h; Cooling with ice; Reflux;
DOI:10.1002/chem.201001794

Reference yield: 91.0%

: 850341-28-5
(S)-6-[(2S,3S,5S)-3-methyl-5-(prop-2-en-1-yl)tetrahydrofuran-2-yl]-2-methylhexanoic acid

: 1259928-75-0
(3R,7R,10S)-10-[(tert-butyldiphenyl)silyl]oxy-7-hydroxy-3-methyl-5-methyleneundec-1-ene

: 1259928-93-2
C₄₄H₆₆O₄Si

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 16h; Cooling with ice;
DOI:10.1002/chem.201001794