8-bromo-7-(2-(3-chlorophenyl)-2-oxoethyl)-3-methyl-1H-purine-2,6(3H,7H)-dione

Base Information

• Chemical Name: 8-bromo-7-(2-(3-chlorophenyl)-2-oxoethyl)-3-methyl-1H-purine-2,6(3H,7H)-dione
• CAS No.: 1415838-41-3
• Molecular Formula: C₁₄H₁₀BrClN₄O₃
• Molecular Weight: 397.615

Synonyms:8-bromo-7-(2-(3-chlorophenyl)-2-oxoethyl)-3-methyl-1H-purine-2,6(3H,7H)-dione

Chemical Property of 8-bromo-7-(2-(3-chlorophenyl)-2-oxoethyl)-3-methyl-1H-purine-2,6(3H,7H)-dione

Chemical Property:

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Technology Process of 8-bromo-7-(2-(3-chlorophenyl)-2-oxoethyl)-3-methyl-1H-purine-2,6(3H,7H)-dione

There total 1 articles about 8-bromo-7-(2-(3-chlorophenyl)-2-oxoethyl)-3-methyl-1H-purine-2,6(3H,7H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

2-bromo-1-(3-chloro-phenyl)-ethanone (41011-01-2) + 3-methyl-8-bromoxanthine (93703-24-3) → 8-bromo-7-(2-(3-chlorophenyl)-2-oxoethyl)-3-methyl-1H-purine-2,6(3H,7H)-dione (1415838-41-3)

Guidance literature:

3-methyl-8-bromoxanthine; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 25 ℃; for 0.0833333h; Inert atmosphere; Schlenk technique;

2-bromo-1-(3-chloro-phenyl)-ethanone; In N,N-dimethyl-formamide; at 25 ℃; for 15h; Inert atmosphere; Schlenk technique;

DOI:10.1021/jm301187e

Reference yield: 45.0%

8-bromo-7-(2-(3-chlorophenyl)-2-oxoethyl)-3-methyl-1H-purine-2,6(3H,7H)-dione (1415838-41-3) + 2-methoxy-phenylamine (90-04-0) → C21H16ClN5O3 (1415838-67-3)

Guidance literature:

In ethanol; at 180 ℃; for 12h; Inert atmosphere; Schlenk technique; Sealed tube;

DOI:10.1021/jm301187e

Reference yield:

8-bromo-7-(2-(3-chlorophenyl)-2-oxoethyl)-3-methyl-1H-purine-2,6(3H,7H)-dione (1415838-41-3) + N-butylamine (109-73-9,85404-21-3) → 8-(butylamino)-7-(2-(butylimino)-2-(3-chlorophenyl)ethyl)-3-methyl-1H-purine-2,6(3H,7H)-dione (1415838-55-9)

Guidance literature:

at 180 ℃; for 0.5h; Inert atmosphere; Schlenk technique;

DOI:10.1021/jm301187e

upstream raw materials:

2-bromo-1-(3-chloro-phenyl)-ethanone

3-methyl-8-bromoxanthine

Downstream raw materials:

8-(butylamino)-7-(2-(butylimino)-2-(3-chlorophenyl)ethyl)-3-methyl-1H-purine-2,6(3H,7H)-dione

C₂₁H₁₆ClN₅O₃

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