methyl c-4-(2¹-naphthyl)-2-(cyclopent-1-enyl)-7-phenyl-6,8-dioxo-3,7-diazabicyclo<3.3.0>octane-r-2-carboxylate

Base Information

• Chemical Name: methyl c-4-(2¹-naphthyl)-2-(cyclopent-1-enyl)-7-phenyl-6,8-dioxo-3,7-diazabicyclo<3.3.0>octane-r-2-carboxylate
• CAS No.: 86774-64-3
• Molecular Formula: C₂₉H₂₆N₂O₄
• Molecular Weight: 466.536

Synonyms:methyl c-4-(2¹-naphthyl)-2-(cyclopent-1-enyl)-7-phenyl-6,8-dioxo-3,7-diazabicyclo<3.3.0>octane-r-2-carboxylate

Chemical Property of methyl c-4-(2¹-naphthyl)-2-(cyclopent-1-enyl)-7-phenyl-6,8-dioxo-3,7-diazabicyclo<3.3.0>octane-r-2-carboxylate

Chemical Property:

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Technology Process of methyl c-4-(2¹-naphthyl)-2-(cyclopent-1-enyl)-7-phenyl-6,8-dioxo-3,7-diazabicyclo<3.3.0>octane-r-2-carboxylate

There total 6 articles about methyl c-4-(2¹-naphthyl)-2-(cyclopent-1-enyl)-7-phenyl-6,8-dioxo-3,7-diazabicyclo<3.3.0>octane-r-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

N-phenyl-maleimide (941-69-5) + Cyclopent-1-enyl-{[1-naphthalen-2-yl-meth-(E)-ylidene]-amino}-acetic acid methyl ester (86774-59-6) → methyl c-4-(21-naphthyl)-2-(cyclopent-1-enyl)-7-phenyl-6,8-dioxo-3,7-diazabicyclo<3.3.0>octane-r-2-carboxylate (86774-64-3)

Guidance literature:

In toluene; at 110 ℃; for 1h;

DOI:10.1016/S0040-4039(00)86404-7

Reference yield: 88.0%

N-phenyl-maleimide (941-69-5) + methyl N-(2-naphthylidene)cyclopent-1-enylglycinate (86774-59-6) → methyl c-4-(21-naphthyl)-2-(cyclopent-1-enyl)-7-phenyl-6,8-dioxo-3,7-diazabicyclo<3.3.0>octane-r-2-carboxylate (86774-64-3)

Guidance literature:

In toluene; at 110 ℃; for 1h;

DOI:10.1016/S0040-4020(01)81969-4

Reference yield:

β-naphthaldehyde (66-99-9) → methyl c-4-(21-naphthyl)-2-(cyclopent-1-enyl)-7-phenyl-6,8-dioxo-3,7-diazabicyclo<3.3.0>octane-r-2-carboxylate (86774-64-3)

Guidance literature:

Multi-step reaction with 2 steps

2: 88 percent / toluene / 1 h / 110 °C

In toluene;

DOI:10.1016/S0040-4039(00)86404-7

upstream raw materials:

N-phenyl-maleimide

methyl N-(2-naphthylidene)cyclopent-1-enylglycinate

Cyclopent-1-enyl-{[1-naphthalen-2-yl-meth-(E)-ylidene]-amino}-acetic acid methyl ester

Amino-cyclopent-1-enyl-acetic acid methyl ester

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