6-N-(2-(5'-O-3'-O-bis(tert-butyldimethylsilyl)-6-O-benzyl-2'-deoxyinosyl))-5'-O-3'-O-bis(tert-butyldimethylsilyl)-2'-deoxyadenosine

Base Information

Chemical Name:6-N-(2-(5'-O-3'-O-bis(tert-butyldimethylsilyl)-6-O-benzyl-2'-deoxyinosyl))-5'-O-3'-O-bis(tert-butyldimethylsilyl)-2'-deoxyadenosine
CAS No.:260798-03-6
Molecular Formula:C₅₁H₈₅N₉O₇Si₄
Molecular Weight:1048.63
Hs Code.:

Synonyms:6-N-(2-(5'-O-3'-O-bis(tert-butyldimethylsilyl)-6-O-benzyl-2'-deoxyinosyl))-5'-O-3'-O-bis(tert-butyldimethylsilyl)-2'-deoxyadenosine

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Chemical Property of 6-N-(2-(5'-O-3'-O-bis(tert-butyldimethylsilyl)-6-O-benzyl-2'-deoxyinosyl))-5'-O-3'-O-bis(tert-butyldimethylsilyl)-2'-deoxyadenosine

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Technology Process of 6-N-(2-(5'-O-3'-O-bis(tert-butyldimethylsilyl)-6-O-benzyl-2'-deoxyinosyl))-5'-O-3'-O-bis(tert-butyldimethylsilyl)-2'-deoxyadenosine

There total 9 articles about 6-N-(2-(5'-O-3'-O-bis(tert-butyldimethylsilyl)-6-O-benzyl-2'-deoxyinosyl))-5'-O-3'-O-bis(tert-butyldimethylsilyl)-2'-deoxyadenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 236427-57-9
O⁶-benzyl-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyguanosine

: 228704-85-6
6-bromo-9-(2-deoxy-3,5-bis-O-(tert-butyldimethylsilyl)-β-D-erythro-pentofuranosyl)purine

: 260798-03-6
6-N-(2-(5'-O-3'-O-bis(tert-butyldimethylsilyl)-6-O-benzyl-2'-deoxyinosyl))-5'-O-3'-O-bis(tert-butyldimethylsilyl)-2'-deoxyadenosine

Guidance literature:: With palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In toluene; at 90 ℃; for 16h;
DOI:10.1021/ol990351m

Reference yield: 47.0%

: 51549-32-7
3',5'-bis-O-[(tert-butyl)dimethylsilyl]-2'-deoxyadenosine

: 236427-57-9
O⁶-benzyl-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyguanosine

: 260798-03-6
6-N-(2-(5'-O-3'-O-bis(tert-butyldimethylsilyl)-6-O-benzyl-2'-deoxyinosyl))-5'-O-3'-O-bis(tert-butyldimethylsilyl)-2'-deoxyadenosine

Guidance literature:: With (R)-2,2'-bis(diphenylphosphanyl)-1,1'-binaphthyl; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In toluene; at 80 ℃; for 2h;
DOI:10.1021/jo991501+

Reference yield: 45.0%

: 135419-06-6
6-iodo-9-[3,5-bis-O-(tert-butyldimethylsilyl)-2-deoxy-β-D-erythro-pentofuranosyl]purine

: 236427-57-9
O⁶-benzyl-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyguanosine

: 260798-03-6
6-N-(2-(5'-O-3'-O-bis(tert-butyldimethylsilyl)-6-O-benzyl-2'-deoxyinosyl))-5'-O-3'-O-bis(tert-butyldimethylsilyl)-2'-deoxyadenosine

: C₇₃H₁₂₃N₁₃O₁₀Si₆

Guidance literature:: With palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In toluene; at 90 ℃; for 16h;
DOI:10.1021/ol990351m