Ethyl 2-cyclohexane-1-carboxylate

Base Information

Chemical Name:Ethyl 2-cyclohexane-1-carboxylate
CAS No.:73453-53-9
Molecular Formula:C₁₉H₂₅NO₄
Molecular Weight:331.412
Hs Code.:

Ethyl 2-<cyano(2,5-dimethoxyphenyl)methyl>cyclohexane-1-carboxylate

Synonyms:Ethyl 2-cyclohexane-1-carboxylate

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Chemical Property of Ethyl 2-cyclohexane-1-carboxylate

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Technology Process of Ethyl 2-cyclohexane-1-carboxylate

There total 3 articles about Ethyl 2-cyclohexane-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 33524-31-1
2,5-dimethoxybenzyl alcohol

: 73453-53-9
Ethyl 2-cyclohexane-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: HCl / benzene

2: NaI / dimethylsulfoxide / 16 h / 90 °C

3: 1) LDA / 1) THF / 1h / -78 deg C 2) 3h / -78 deg C; 3h / 0 deg C

With hydrogenchloride; sodium iodide; lithium diisopropyl amide; In dimethyl sulfoxide; benzene;
DOI:10.1021/jo01301a015

Reference yield:

: 3840-27-5
2,5-dimethoxybenzyl chloride

: 73453-53-9
Ethyl 2-cyclohexane-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: NaI / dimethylsulfoxide / 16 h / 90 °C

2: 1) LDA / 1) THF / 1h / -78 deg C 2) 3h / -78 deg C; 3h / 0 deg C

With sodium iodide; lithium diisopropyl amide; In dimethyl sulfoxide;
DOI:10.1021/jo01301a015

Reference yield:

: 71911-74-5
Ethyl 1-chlorocyclohexane-1-carboxylate

: 73453-53-9
Ethyl 2-cyclohexane-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / NEt₃ / ethanol / 14 h / Heating

2: 1) LDA / 1) THF / 1h / -78 deg C 2) 3h / -78 deg C; 3h / 0 deg C

With triethylamine; lithium diisopropyl amide; In ethanol;
DOI:10.1021/jo01301a015