11-(4-hydroxyphenyl)-13-methyl-8,17-dioxa-14,15-diazatetracyclo[8.7.0.0(2,7).0(12,16)]heptadeca-1⁽¹⁰⁾,2⁽⁷⁾,3,5,12⁽¹⁶⁾,13-hexaen-9-one

Base Information

• Chemical Name: 11-(4-hydroxyphenyl)-13-methyl-8,17-dioxa-14,15-diazatetracyclo[8.7.0.0(2,7).0(12,16)]heptadeca-1⁽¹⁰⁾,2⁽⁷⁾,3,5,12⁽¹⁶⁾,13-hexaen-9-one
• CAS No.: 1299494-31-7
• Molecular Formula: C₂₀H₁₄N₂O₄
• Molecular Weight: 346.342

Synonyms:11-(4-hydroxyphenyl)-13-methyl-8,17-dioxa-14,15-diazatetracyclo[8.7.0.0(2,7).0(12,16)]heptadeca-1⁽¹⁰⁾,2⁽⁷⁾,3,5,12⁽¹⁶⁾,13-hexaen-9-one

Chemical Property of 11-(4-hydroxyphenyl)-13-methyl-8,17-dioxa-14,15-diazatetracyclo[8.7.0.0(2,7).0(12,16)]heptadeca-1⁽¹⁰⁾,2⁽⁷⁾,3,5,12⁽¹⁶⁾,13-hexaen-9-one

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Technology Process of 11-(4-hydroxyphenyl)-13-methyl-8,17-dioxa-14,15-diazatetracyclo[8.7.0.0(2,7).0(12,16)]heptadeca-1⁽¹⁰⁾,2⁽⁷⁾,3,5,12⁽¹⁶⁾,13-hexaen-9-one

There total 2 articles about 11-(4-hydroxyphenyl)-13-methyl-8,17-dioxa-14,15-diazatetracyclo[8.7.0.0(2,7).0(12,16)]heptadeca-1⁽¹⁰⁾,2⁽⁷⁾,3,5,12⁽¹⁶⁾,13-hexaen-9-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

4-hydroxy[1]benzopyran-2-one (1076-38-6,92395-12-5) + ethyl acetoacetate (141-97-9) + 4-hydroxy-benzaldehyde (123-08-0,65581-83-1) → 11-(4-hydroxyphenyl)-13-methyl-8,17-dioxa-14,15-diazatetracyclo[8.7.0.0(2,7).0(12,16)]heptadeca-1(10),2(7),3,5,12(16),13-hexaen-9-one (1299494-31-7)

Guidance literature:

With hydrazine hydrate; In ethanol; water; for 4h; chemoselective reaction; Reflux; Green chemistry;

DOI:10.1007/s13738-016-0949-0

Reference yield: 80.0%

4-hydroxy[1]benzopyran-2-one (1076-38-6,92395-12-5) + 4-hydroxy-benzaldehyde (123-08-0,65581-83-1) + 3-methyl-2-pyrazoline-5-one (108-26-9) → 11-(4-hydroxyphenyl)-13-methyl-8,17-dioxa-14,15-diazatetracyclo[8.7.0.0(2,7).0(12,16)]heptadeca-1(10),2(7),3,5,12(16),13-hexaen-9-one (1299494-31-7)

Guidance literature:

With aminosulfonic acid; In acetonitrile; for 4.5h; chemoselective reaction; Reflux;

DOI:10.3987/COM-10-12036

upstream raw materials:

4-hydroxy[1]benzopyran-2-one

4-hydroxy-benzaldehyde

3-methyl-2-pyrazoline-5-one

ethyl acetoacetate

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