(2-ethyl)bistrifluoromethyl thiophenolmethylphosphoric acid ethyl ester

Base Information

• Chemical Name: (2-ethyl)bistrifluoromethyl thiophenolmethylphosphoric acid ethyl ester
• CAS No.: 934177-56-7
• Molecular Formula: C₁₃H₁₅F₆O₃PS
• Molecular Weight: 396.29
• Mol file: 934177-56-7.mol

Synonyms:(2-ethyl)bistrifluoromethyl thiophenolmethylphosphoric acid ethyl ester

Chemical Property of (2-ethyl)bistrifluoromethyl thiophenolmethylphosphoric acid ethyl ester

Chemical Property:

Purity/Quality:

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Technology Process of (2-ethyl)bistrifluoromethyl thiophenolmethylphosphoric acid ethyl ester

There total 2 articles about (2-ethyl)bistrifluoromethyl thiophenolmethylphosphoric acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

diethyl (p-toluenesulfonyloxymethane)phosphonate (31618-90-3) + 3,5-bis(trifluoromethyl)thiophenol (130783-02-7) → (2-ethyl)bistrifluoromethyl thiophenolmethylphosphoric acid ethyl ester (934177-56-7)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 5h;

DOI:10.1021/acs.jmedchem.9b01663

Reference yield: 90.0%

diethyl iodomethanephosphonate (10419-77-9) + 3,5-bis(trifluoromethyl)thiophenol (130783-02-7) → (2-ethyl)bistrifluoromethyl thiophenolmethylphosphoric acid ethyl ester (934177-56-7)

Guidance literature:

With sodium hydride; In acetonitrile; at 20 ℃; for 24h;

DOI:10.1016/j.tetasy.2010.03.043

Reference yield: 90.0%

(2-ethyl)bistrifluoromethyl thiophenolmethylphosphoric acid ethyl ester (934177-56-7) → C13H15F6O4PS

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In chloroform; at 20 ℃;

upstream raw materials:

diethyl iodomethanephosphonate

3,5-bis(trifluoromethyl)thiophenol

diethyl (p-toluenesulfonyloxymethane)phosphonate

Downstream raw materials:

C₁₃H₁₅F₆O₅PS