9-benzyl-3-((N-(2,2-diethoxyethyl)-N-tosylamino)methyl)-1,4-dimethylcarbazole

Base Information

Chemical Name:9-benzyl-3-((N-(2,2-diethoxyethyl)-N-tosylamino)methyl)-1,4-dimethylcarbazole
CAS No.:129868-41-3
Molecular Formula:C₃₅H₄₀N₂O₄S
Molecular Weight:584.78
Hs Code.:

Synonyms:9-benzyl-3-((N-(2,2-diethoxyethyl)-N-tosylamino)methyl)-1,4-dimethylcarbazole

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Chemical Property of 9-benzyl-3-((N-(2,2-diethoxyethyl)-N-tosylamino)methyl)-1,4-dimethylcarbazole

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Technology Process of 9-benzyl-3-((N-(2,2-diethoxyethyl)-N-tosylamino)methyl)-1,4-dimethylcarbazole

There total 11 articles about 9-benzyl-3-((N-(2,2-diethoxyethyl)-N-tosylamino)methyl)-1,4-dimethylcarbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 129868-47-9
9-benzyl-1-((N,N-dimethylamino)methyl)-4-methylcarbazole-3-carbaldehyde

: 129868-41-3
9-benzyl-3-((N-(2,2-diethoxyethyl)-N-tosylamino)methyl)-1,4-dimethylcarbazole

Guidance literature:: Multi-step reaction with 4 steps

1: 3 h / Heating

2: H₂ / 10percent Pd-C / ethanol / 9.5 h / 80 °C

3: 81 percent / 2 h / 100 °C

4: 1.) NaBH₄ 2.) Na₂CO₃ / 1.) MeOH, RT, 2 h 2.) THF-water, RT, 1.5 h

With sodium tetrahydroborate; hydrogen; sodium carbonate; palladium on activated charcoal; In ethanol;

Reference yield:

: 129868-52-6
(9-Benzyl-3-formyl-4-methyl-9H-carbazol-1-ylmethyl)-trimethyl-ammonium; iodide

: 129868-41-3
9-benzyl-3-((N-(2,2-diethoxyethyl)-N-tosylamino)methyl)-1,4-dimethylcarbazole

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / 10percent Pd-C / ethanol / 9.5 h / 80 °C

2: 81 percent / 2 h / 100 °C

3: 1.) NaBH₄ 2.) Na₂CO₃ / 1.) MeOH, RT, 2 h 2.) THF-water, RT, 1.5 h

With sodium tetrahydroborate; hydrogen; sodium carbonate; palladium on activated charcoal; In ethanol;

Reference yield:

: 19283-46-6
(Z)-4-methylcyclohexane-1,2-dione 2-phenylhydrazone

: 129868-41-3
9-benzyl-3-((N-(2,2-diethoxyethyl)-N-tosylamino)methyl)-1,4-dimethylcarbazole

Guidance literature:: Multi-step reaction with 7 steps

1: 85 percent / PTSA / benzene / 2.5 h / Ambient temperature

2: 1.) hydrazine hydrate, KOH, triethylene glycol 2.) KOH / 1.) a) 150 deg C, 2 h b) 200 deg C, 2,5 h 2.) DMSO, RT

3: 88 percent / POCl₃ / 6 h / 0 °C

4: 43 percent / POCl₃ / 2 h / 60 °C

5: POCl₃ / 6 h / 100 °C

6: 81 percent / 2 h / 100 °C

7: 1.) NaBH₄ 2.) Na₂CO₃ / 1.) MeOH, RT, 2 h 2.) THF-water, RT, 1.5 h

With potassium hydroxide; sodium tetrahydroborate; sodium carbonate; toluene-4-sulfonic acid; hydrazine hydrate; trichlorophosphate; 2,2'-[1,2-ethanediylbis(oxy)]bisethanol; In benzene;