3-(benzylamino)-4,4,4-trifluorobutanoic acid

Base Information

• Chemical Name: 3-(benzylamino)-4,4,4-trifluorobutanoic acid
• CAS No.: 1022990-69-7
• Molecular Formula: C₁₁H₁₂F₃NO₂
• Molecular Weight: 247.217
• Mol file: 1022990-69-7.mol

Synonyms:3-(benzylamino)-4,4,4-trifluorobutanoic acid

Chemical Property of 3-(benzylamino)-4,4,4-trifluorobutanoic acid

Chemical Property:

Purity/Quality:

3-(benzylamino)-4,4,4-trifluorobutanoicacid 95 ^*data from reagent suppliers

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Technology Process of 3-(benzylamino)-4,4,4-trifluorobutanoic acid

There total 1 articles about 3-(benzylamino)-4,4,4-trifluorobutanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

ethyl 3-(benzylamino)-4,4,4-trifluorobutanoate (247134-05-0) → 3-(benzylamino)-4,4,4-trifluorobutanoic acid (1022990-69-7)

Guidance literature:

With sodium hydroxide; In isopropyl alcohol; at 0 - 20 ℃;

DOI:10.1016/j.jfluchem.2007.03.007

Reference yield: 78.0%

3-(benzylamino)-4,4,4-trifluorobutanoic acid (1022990-69-7) + glycine ethyl ester hydrochloride (5680-79-5,883886-67-7) → methyl 2-[3-(benzylamino)-4,4,4-trifluorobutanamido]acetate

Guidance literature:

3-(benzylamino)-4,4,4-trifluorobutanoic acid; With 2-chloro-1-methyl-pyridinium iodide; In dimethyl sulfoxide; at 20 ℃; for 0.25h;

glycine ethyl ester hydrochloride; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; Further stages.;

DOI:10.1016/j.jfluchem.2007.03.007

Reference yield:

3-(benzylamino)-4,4,4-trifluorobutanoic acid (1022990-69-7) → 3-(benzylamino)-4,4,4-trifluorobutanoyl chloride

Guidance literature:

With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1016/j.jfluchem.2007.03.007

upstream raw materials:

ethyl 3-(benzylamino)-4,4,4-trifluorobutanoate

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