1-(3,5-bis(N-benzyl-5'-dimethylaminonaphthalene-1'-sulfonamido)benzyl)-1,4,8,11-tetraazacyclotetradecane

Base Information

Chemical Name:1-(3,5-bis(N-benzyl-5'-dimethylaminonaphthalene-1'-sulfonamido)benzyl)-1,4,8,11-tetraazacyclotetradecane
CAS No.:1246274-97-4
Molecular Formula:C₅₅H₆₆N₈O₄S₂
Molecular Weight:967.312
Hs Code.:

Synonyms:1-(3,5-bis(N-benzyl-5'-dimethylaminonaphthalene-1'-sulfonamido)benzyl)-1,4,8,11-tetraazacyclotetradecane

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Chemical Property of 1-(3,5-bis(N-benzyl-5'-dimethylaminonaphthalene-1'-sulfonamido)benzyl)-1,4,8,11-tetraazacyclotetradecane

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Technology Process of 1-(3,5-bis(N-benzyl-5'-dimethylaminonaphthalene-1'-sulfonamido)benzyl)-1,4,8,11-tetraazacyclotetradecane

There total 7 articles about 1-(3,5-bis(N-benzyl-5'-dimethylaminonaphthalene-1'-sulfonamido)benzyl)-1,4,8,11-tetraazacyclotetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3,5-bis(5'-dimethylaminonaphthalene-1'-sulfonamido)benzyl alcohol

: 1246274-97-4
1-(3,5-bis(N-benzyl-5'-dimethylaminonaphthalene-1'-sulfonamido)benzyl)-1,4,8,11-tetraazacyclotetradecane

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide / 72 h / 20 °C

2: carbon tetrabromide; triphenylphosphine / tetrahydrofuran / 0.33 h / Inert atmosphere

3: potassium carbonate / N,N-dimethyl-formamide / 72 h / 20 °C

4: water; sodium carbonate / methanol / 3 h / Reflux

With carbon tetrabromide; water; sodium carbonate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1002/asia.201000170

Reference yield:

: 295-37-4
1,4,8,11-Tetraazacyclotetradecane

: 1246274-97-4
1-(3,5-bis(N-benzyl-5'-dimethylaminonaphthalene-1'-sulfonamido)benzyl)-1,4,8,11-tetraazacyclotetradecane

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / methanol / 5 h / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 72 h / 20 °C

3: water; sodium carbonate / methanol / 3 h / Reflux

With water; sodium carbonate; potassium carbonate; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1002/asia.201000170

Reference yield:

: 1246274-91-8
3,5-bis(N-benzyl-5'-dimethylaminonaphthalene-1'-sulfonamido)benzyl alcohol

: 1246274-97-4
1-(3,5-bis(N-benzyl-5'-dimethylaminonaphthalene-1'-sulfonamido)benzyl)-1,4,8,11-tetraazacyclotetradecane

Guidance literature:: Multi-step reaction with 3 steps

1: carbon tetrabromide; triphenylphosphine / tetrahydrofuran / 0.33 h / Inert atmosphere

2: potassium carbonate / N,N-dimethyl-formamide / 72 h / 20 °C

3: water; sodium carbonate / methanol / 3 h / Reflux

With carbon tetrabromide; water; sodium carbonate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1002/asia.201000170