dibenzyl 7-(propan-2-ylidene)-3,3a,7,7a-tetrahydro-1H-indene-2,2(6H)-dicarboxylate

Base Information

Chemical Name:dibenzyl 7-(propan-2-ylidene)-3,3a,7,7a-tetrahydro-1H-indene-2,2(6H)-dicarboxylate
CAS No.:1398654-02-8
Molecular Formula:C₂₈H₃₀O₄
Molecular Weight:430.544
Hs Code.:

Synonyms:dibenzyl 7-(propan-2-ylidene)-3,3a,7,7a-tetrahydro-1H-indene-2,2(6H)-dicarboxylate

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Chemical Property of dibenzyl 7-(propan-2-ylidene)-3,3a,7,7a-tetrahydro-1H-indene-2,2(6H)-dicarboxylate

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Technology Process of dibenzyl 7-(propan-2-ylidene)-3,3a,7,7a-tetrahydro-1H-indene-2,2(6H)-dicarboxylate

There total 2 articles about dibenzyl 7-(propan-2-ylidene)-3,3a,7,7a-tetrahydro-1H-indene-2,2(6H)-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: C₂₈H₃₀O₄

: 1398654-02-8
dibenzyl 7-(propan-2-ylidene)-3,3a,7,7a-tetrahydro-1H-indene-2,2(6H)-dicarboxylate

: dibenzyl 7-(propan-2-ylidene)-3,3a,7,7a-tetrahydro-1H-indene-2,2(6H)-dicarboxylate

Guidance literature:: With silver tetrafluoroborate; C₅₀H₅₄AuClNO₄P; In dichloromethane; at 0 - 20 ℃; for 1.91667h; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja303641p

Reference yield:

: 1202790-20-2
dibenzyl (4-methylpenta-2,3-dien-1-yl)[(2E)-penta-2,4-dien-1-yl]propanedioate

: 1398654-02-8
dibenzyl 7-(propan-2-ylidene)-3,3a,7,7a-tetrahydro-1H-indene-2,2(6H)-dicarboxylate

: dibenzyl 7-(propan-2-ylidene)-3,3a,7,7a-tetrahydro-1H-indene-2,2(6H)-dicarboxylate

Guidance literature:: With AgBF₄; C₉₃H₁₀₅AuClO₉P; In dichloromethane; at -30 ℃; for 24h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ol902622b