C₁₁H₁₃FO₅S

Base Information

Chemical Name:C₁₁H₁₃FO₅S
CAS No.:1402742-03-3
Molecular Formula:C₁₁H₁₃FO₅S
Molecular Weight:276.286
Hs Code.:

C<sub>11</sub>H<sub>13</sub>FO<sub>5</sub>S

Synonyms:C₁₁H₁₃FO₅S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₁H₁₃FO₅S

Chemical Property:

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Technology Process of C₁₁H₁₃FO₅S

There total 1 articles about C₁₁H₁₃FO₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1259524-13-4
ethyl 2-(2-fluorophenyl)acrylate

: 1402742-03-3
C₁₁H₁₃FO₅S

Guidance literature:: With sodium hydrogensulfite; In ethanol; water; at 165 ℃; for 0.5h; microwave reactor;

Reference yield:

: 1402742-03-3
C₁₁H₁₃FO₅S

: 1402742-04-4
C₁₁H₁₂ClFO₄S

Guidance literature:: With thionyl chloride; for 3h; Reflux;

Reference yield:

: 1402742-03-3
C₁₁H₁₃FO₅S

: C₁₉H₂₃FN₂O₄S

Guidance literature:: Multi-step reaction with 8 steps

1.1: thionyl chloride / 3 h / Reflux

2.1: triethylamine / dichloromethane / 3 h / 0 - 25 °C

3.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C

4.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 - -30 °C

4.2: -78 - 25 °C

5.1: hydrogen / palladium hydrogenation catalyst / ethanol

6.1: diethoxyltriphenylphosphorane / toluene / 60 h / 45 °C

7.1: water; lithium hydroxide / tetrahydrofuran / 60 °C

7.2: 25 °C / pH 3

8.1: triethylamine; diphenyl phosphoryl azide / tetrahydrofuran / 24 h / 25 °C

8.2: 1.5 h / 80 °C

With thionyl chloride; diphenyl phosphoryl azide; diethoxyltriphenylphosphorane; water; hydrogen; sodium hexamethyldisilazane; triethylamine; lithium hydroxide; lithium diisopropyl amide; palladium hydrogenation catalyst; In tetrahydrofuran; ethanol; dichloromethane; toluene;