C₂₉H₄₀N₂O₅

Base Information

Chemical Name:C₂₉H₄₀N₂O₅
CAS No.:1262516-01-7
Molecular Formula:C₂₉H₄₀N₂O₅
Molecular Weight:496.647
Hs Code.:

C<sub>29</sub>H<sub>40</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₂₉H₄₀N₂O₅

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Chemical Property of C₂₉H₄₀N₂O₅

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Technology Process of C₂₉H₄₀N₂O₅

There total 6 articles about C₂₉H₄₀N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1262515-92-3
3''-pentyl (3S,5R,αS)-3-[N-benzyl-N-(α-methylbenzyl)amino]-4-[2',2';-dimethyl-N(3')-tert-butoxycarbonyl-1',3'-oxazolidin-5'-yl]butanoate

: 1262516-01-7
C₂₉H₄₀N₂O₅

Guidance literature:: 3''-pentyl (3S,5R,αS)-3-[N-benzyl-N-(α-methylbenzyl)amino]-4-[2',2';-dimethyl-N(3')-tert-butoxycarbonyl-1',3'-oxazolidin-5'-yl]butanoate; With lithium hydroxide monohydrate; water; In tetrahydrofuran; methanol; for 24h; Reflux;

With hydrogenchloride; In tetrahydrofuran; methanol; water; at 20 ℃; pH=6;
DOI:10.1016/j.tet.2010.10.067

Reference yield:

: 181772-82-7
(R)-2-[2',2'-dimethyl-N(3')-tert-butoxycarbonyl-1',3'-oxazolidin-5'-yl]ethanol

: 1262516-01-7
C₂₉H₄₀N₂O₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.25 h / -63 °C / Inert atmosphere

1.2: -63 - 20 °C / Inert atmosphere

2.1: toluene / 4 h / 70 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C / Inert atmosphere

3.2: 1 h / -78 °C / Inert atmosphere

4.1: lithium hydroxide monohydrate; water / tetrahydrofuran; methanol / 24 h / Reflux

4.2: 20 °C / pH 6

With n-butyllithium; oxalyl dichloride; lithium hydroxide monohydrate; water; dimethyl sulfoxide; In tetrahydrofuran; methanol; hexane; dichloromethane; toluene; 1.1: Swern oxidation / 1.2: Swern oxidation / 2.1: Wittig reaction;
DOI:10.1016/j.tet.2010.10.067

Reference yield:

: 181772-51-0
ethyl (3R)-4-(tert-butyloxycarbonyl)amino-3-hydroxybutanoate

: 1262516-01-7
C₂₉H₄₀N₂O₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: (R)-10-camphorsulfonic acid / acetone / 2 h / 70 °C / Inert atmosphere

2.1: sodium bis(2-methoxyethoxy)aluminium dihydride / toluene / 1 h / 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.25 h / -63 °C / Inert atmosphere

3.2: -63 - 20 °C / Inert atmosphere

4.1: toluene / 4 h / 70 °C / Inert atmosphere

5.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C / Inert atmosphere

5.2: 1 h / -78 °C / Inert atmosphere

6.1: lithium hydroxide monohydrate; water / tetrahydrofuran; methanol / 24 h / Reflux

6.2: 20 °C / pH 6

With n-butyllithium; oxalyl dichloride; lithium hydroxide monohydrate; (R)-10-camphorsulfonic acid; water; dimethyl sulfoxide; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; methanol; hexane; dichloromethane; acetone; toluene; 3.1: Swern oxidation / 3.2: Swern oxidation / 4.1: Wittig reaction;
DOI:10.1016/j.tet.2010.10.067