N-<4-(dimethylamino)phenyl>-α-<6-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)pyridazin-3-yl>nitrone

Base Information

Chemical Name:N-<4-(dimethylamino)phenyl>-α-<6-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)pyridazin-3-yl>nitrone
CAS No.:135195-61-8
Molecular Formula:C₃₉H₃₄N₄O₈
Molecular Weight:686.721
Hs Code.:

Synonyms:N-<4-(dimethylamino)phenyl>-α-<6-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)pyridazin-3-yl>nitrone

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Chemical Property of N-<4-(dimethylamino)phenyl>-α-<6-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)pyridazin-3-yl>nitrone

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Technology Process of N-<4-(dimethylamino)phenyl>-α-<6-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)pyridazin-3-yl>nitrone

There total 3 articles about N-<4-(dimethylamino)phenyl>-α-<6-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)pyridazin-3-yl>nitrone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121701-32-4
6-hydroxy-6-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)pyran-3<2H,6H>-one

: 135195-61-8
N-<4-(dimethylamino)phenyl>-α-<6-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)pyridazin-3-yl>nitrone

Guidance literature:: Multi-step reaction with 3 steps

1: 58.3 percent / anhydrous hydrazine / dioxane / 0.5 h / Ambient temperature

2: 73.5 percent / thionyl bromid / benzene / 1 h / Ambient temperature

3: 2) aq. Na₂CO₃ / 1) pyridine, 1h, r.t., 2) methanol, 1h

With dibromo sulfoxide; sodium carbonate; hydrazine; In 1,4-dioxane; benzene;

Reference yield:

: 135195-58-3
3-hydroxymethyl-6-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)pyridazine

: 135195-61-8
N-<4-(dimethylamino)phenyl>-α-<6-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)pyridazin-3-yl>nitrone

Guidance literature:: Multi-step reaction with 2 steps

1: 73.5 percent / thionyl bromid / benzene / 1 h / Ambient temperature

2: 2) aq. Na₂CO₃ / 1) pyridine, 1h, r.t., 2) methanol, 1h

With dibromo sulfoxide; sodium carbonate; In benzene;