N-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-N-(10-cyano-1-propyl-dec-6-enyl)-4-methyl-benzenesulfonamide

Base Information

• Chemical Name: N-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-N-(10-cyano-1-propyl-dec-6-enyl)-4-methyl-benzenesulfonamide
• CAS No.: 718606-52-1
• Molecular Formula: C₂₉H₅₀N₂O₃SSi
• Molecular Weight: 534.879

Synonyms:N-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-N-(10-cyano-1-propyl-dec-6-enyl)-4-methyl-benzenesulfonamide

Chemical Property of N-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-N-(10-cyano-1-propyl-dec-6-enyl)-4-methyl-benzenesulfonamide

Chemical Property:

Purity/Quality:

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Technology Process of N-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-N-(10-cyano-1-propyl-dec-6-enyl)-4-methyl-benzenesulfonamide

There total 3 articles about N-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-N-(10-cyano-1-propyl-dec-6-enyl)-4-methyl-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

N-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-4-methyl-benzenesulfonamide (202974-92-3) + (Z)-(S)-11-Hydroxy-tetradec-5-enenitrile → N-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-N-(10-cyano-1-propyl-dec-6-enyl)-4-methyl-benzenesulfonamide (718606-52-1)

Guidance literature:

With (trimethyl-λ5-phosphanyliden)acetonitrile; In toluene; at 20 ℃; for 24h;

DOI:10.1246/cl.2004.516

Reference yield:

(4-cyanobutyl)triphenylphosphonium bromide (7743-27-3) → N-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-N-(10-cyano-1-propyl-dec-6-enyl)-4-methyl-benzenesulfonamide (718606-52-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: DIBAL / CH₂Cl₂

1.2: 70 percent / sodium dimsylate / dimethylsulfoxide / 0.5 h / 20 °C

2.1: 91 percent / cyanomethylenetrimethylphosphorane / toluene / 24 h / 20 °C

With diisobutylaluminium hydride; (trimethyl-λ5-phosphanyliden)acetonitrile; In dichloromethane; toluene; 1.2: Wittig reaction / 2.1: Walden inversion;

DOI:10.1246/cl.2004.516

Reference yield:

7-propyl-2-oxepanone (115510-47-9) → N-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-N-(10-cyano-1-propyl-dec-6-enyl)-4-methyl-benzenesulfonamide (718606-52-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: DIBAL / CH₂Cl₂

1.2: 70 percent / sodium dimsylate / dimethylsulfoxide / 0.5 h / 20 °C

2.1: 91 percent / cyanomethylenetrimethylphosphorane / toluene / 24 h / 20 °C

With diisobutylaluminium hydride; (trimethyl-λ5-phosphanyliden)acetonitrile; In dichloromethane; toluene; 1.2: Wittig reaction / 2.1: Walden inversion;

DOI:10.1246/cl.2004.516

upstream raw materials:

N-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-4-methyl-benzenesulfonamide

(4-cyanobutyl)triphenylphosphonium bromide

7-propyl-2-oxepanone

Downstream raw materials:

(Z)-(R)-5-Propyl-4-(toluene-4-sulfonyl)-1-oxa-4-aza-cyclopentadec-10-en-15-one

(R)-(-)-epilachnene

(Z)-(R)-11-[(2-Hydroxy-ethyl)-(toluene-4-sulfonyl)-amino]-tetradec-5-enoic acid

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