5-{5-[2,6-dimethyl-4-(2-methoxycarbonylmethyl-2H-tetrazol-5-yl)phenoxy]pentyl}-3-methylisoxazole

Base Information

Chemical Name:5-{5-[2,6-dimethyl-4-(2-methoxycarbonylmethyl-2H-tetrazol-5-yl)phenoxy]pentyl}-3-methylisoxazole
CAS No.:126225-53-4
Molecular Formula:C₂₁H₂₇N₅O₄
Molecular Weight:413.476
Hs Code.:

Synonyms:5-{5-[2,6-dimethyl-4-(2-methoxycarbonylmethyl-2H-tetrazol-5-yl)phenoxy]pentyl}-3-methylisoxazole

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Chemical Property of 5-{5-[2,6-dimethyl-4-(2-methoxycarbonylmethyl-2H-tetrazol-5-yl)phenoxy]pentyl}-3-methylisoxazole

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Technology Process of 5-{5-[2,6-dimethyl-4-(2-methoxycarbonylmethyl-2H-tetrazol-5-yl)phenoxy]pentyl}-3-methylisoxazole

There total 7 articles about 5-{5-[2,6-dimethyl-4-(2-methoxycarbonylmethyl-2H-tetrazol-5-yl)phenoxy]pentyl}-3-methylisoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 5-{5-[2,6-dimethyl-4-(1H-tetrazol-5-yl)phenoxy]pentyl}-3-methylisoxazole

: 96-32-2
bromoacetic acid methyl ester

: 126225-53-4
5-{5-[2,6-dimethyl-4-(2-methoxycarbonylmethyl-2H-tetrazol-5-yl)phenoxy]pentyl}-3-methylisoxazole

Guidance literature:: potassium carbonate;

Reference yield:

: 126225-60-3
5-<3,5-dimethyl-4-<<5-(3-methyl-5-isoxazolyl)pentyl>oxy>phenyl>-2H-tetrazole

: 126225-53-4
5-{5-[2,6-dimethyl-4-(2-methoxycarbonylmethyl-2H-tetrazol-5-yl)phenoxy]pentyl}-3-methylisoxazole

Guidance literature:: With potassium carbonate; In acetonitrile; for 1h; Heating;
DOI:10.1021/jm00074a004

Reference yield:

: 2233-18-3
4-hydroxy-3,5-dimethylbenzaldehyde

: 126225-53-4
5-{5-[2,6-dimethyl-4-(2-methoxycarbonylmethyl-2H-tetrazol-5-yl)phenoxy]pentyl}-3-methylisoxazole

Guidance literature:: Multi-step reaction with 5 steps

1: 82 percent / K₂CO₃ / acetonitrile / 5 h / Heating

2: 85 percent / NH₂OH*HCl / pyridine / 1 h / Heating

3: 86 percent / Ac₂O / 12 h / Heating

4: 93 percent / NaN₃, NH₄Cl / dimethylformamide / 72 h / 100 °C

5: K₂CO₃ / acetonitrile / 1 h / Heating

With sodium azide; hydroxylamine hydrochloride; acetic anhydride; potassium carbonate; ammonium chloride; In pyridine; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm00074a004