C₄₉H₇₂BrN₃O₁₀Si₂

Base Information

Chemical Name:C₄₉H₇₂BrN₃O₁₀Si₂
CAS No.:1310875-43-4
Molecular Formula:C₄₉H₇₂BrN₃O₁₀Si₂
Molecular Weight:999.2
Hs Code.:

C<sub>49</sub>H<sub>72</sub>BrN<sub>3</sub>O<sub>10</sub>Si<sub>2</sub>

Synonyms:C₄₉H₇₂BrN₃O₁₀Si₂

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Chemical Property of C₄₉H₇₂BrN₃O₁₀Si₂

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Technology Process of C₄₉H₇₂BrN₃O₁₀Si₂

There total 6 articles about C₄₉H₇₂BrN₃O₁₀Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1310875-42-3
C₄₉H₇₄BrN₃O₁₀Si₂

: 1310875-43-4
C₄₉H₇₂BrN₃O₁₀Si₂

Guidance literature:: With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1021/jo200758r

Reference yield:

: 1310875-41-2
C₅₅H₈₈BrN₃O₁₀Si₃

: 1310875-43-4
C₄₉H₇₂BrN₃O₁₀Si₂

Guidance literature:: Multi-step reaction with 2 steps

1: formic acid / tetrahydrofuran; water / 10 h / 20 °C

2: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 2 h / 20 °C

With formic acid; sodium hydrogencarbonate; Dess-Martin periodane; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/jo200758r

Reference yield:

: 686776-27-2
(S)-5-(2-amino-3-hydroxypropyl)-2-methoxy-3-methylphenol

: 1310875-43-4
C₄₉H₇₂BrN₃O₁₀Si₂

Guidance literature:: Multi-step reaction with 5 steps

1: acetic acid / dichloromethane; 2,2,2-trifluoroethanol / 10 h / 0 °C / Inert atmosphere; Molecular sieve

2: 1H-imidazole / N,N-dimethyl-formamide / 48 h / 20 °C / Inert atmosphere

3: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine / dichloromethane / 72 h / 20 °C / Cooling with ice

4: formic acid / tetrahydrofuran; water / 10 h / 20 °C

5: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 2 h / 20 °C

With 1H-imidazole; formic acid; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; sodium hydrogencarbonate; Dess-Martin periodane; acetic acid; triethylamine; In tetrahydrofuran; dichloromethane; 2,2,2-trifluoroethanol; water; N,N-dimethyl-formamide; 1: Pictet-Spengler cyclisation;
DOI:10.1021/jo200758r