Technology Process of C24H27NO3Se
There total 7 articles about C24H27NO3Se which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium cyanoborohydride;
In
tetrahydrofuran; methanol;
DOI:10.1021/ja00237a057
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1) Me3SiOTf, Et3N, 2) Pd(II)acetate / 1) CH2Cl2, 2) CH3CN, 25 deg C, 14 h
2: 1) KH, 2) n-BuLi / 1) THF, 25 deg C, 2) THF, -78 deg C, 3) THF, -78 deg C to -30 deg C, 10 h
3: MeSiOTf / CH2Cl2 / 10 h / -78 °C
4: 95 percent / DBU
5: 45 percent / NaCNBH3 / tetrahydrofuran; methanol
With
n-butyllithium; trimethylsilyl trifluoromethanesulfonate; MeSiOTf; palladium diacetate; potassium hydride; sodium cyanoborohydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ja00237a057
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1) KH, 2) n-BuLi / 1) THF, 25 deg C, 2) THF, -78 deg C, 3) THF, -78 deg C to -30 deg C, 10 h
2: MeSiOTf / CH2Cl2 / 10 h / -78 °C
3: 95 percent / DBU
4: 45 percent / NaCNBH3 / tetrahydrofuran; methanol
With
n-butyllithium; MeSiOTf; potassium hydride; sodium cyanoborohydride; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ja00237a057
