(E)-1-methyl-4-(4-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)benzyl)piperazine

Base Information

Chemical Name:(E)-1-methyl-4-(4-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)benzyl)piperazine
CAS No.:933986-41-5
Molecular Formula:C₂₀H₃₁BN₂O₂
Molecular Weight:342.289
Hs Code.:

Synonyms:(E)-1-methyl-4-(4-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)benzyl)piperazine

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Chemical Property of (E)-1-methyl-4-(4-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)benzyl)piperazine

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Technology Process of (E)-1-methyl-4-(4-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)benzyl)piperazine

There total 1 articles about (E)-1-methyl-4-(4-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)benzyl)piperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 368879-17-8
4-[(4-methylpiperazin-1-yl)methyl]bromobenzene

: 75927-49-0
pinacol vinylboronate

: 933986-41-5
(E)-1-methyl-4-(4-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)benzyl)piperazine

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-ethyl-N,N-diisopropylamine; tri tert-butylphosphoniumtetrafluoroborate; In toluene; at 95 ℃; for 3h; Inert atmosphere;
DOI:10.1039/C6NJ03984G

Reference yield:

: 933986-16-4
6-(2-chloro-pyridin-4-yl)-3,7-dihydro-pyrrolo[2,3-d]pyrimidin-4-one

: 933986-41-5
(E)-1-methyl-4-(4-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)benzyl)piperazine

: 6-(2-{(E)-2-[4-(4-methyl-piperazin-1ylmethyl)-phenyl]-vinyl}-pyridin-4-yl)-3,7-dihydro-pyrrolo[2,3-d]pyrimidine-one

Guidance literature:: With sodium carbonate; bis-triphenylphosphine-palladium(II) chloride; In propan-1-ol; water; at 140 ℃; for 0.25h; Microwave irradiation;

Reference yield:

: 933986-41-5
(E)-1-methyl-4-(4-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)benzyl)piperazine

: 4-(3-iodo-1H-indazol-6-yl)pyrimidin-2-amine

: C₂₅H₂₇N₇

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate; In 1,4-dioxane; water; at 100 ℃; for 8h;
DOI:10.1039/c7ra02518a