4-(1-azido-2-iodoethyl)benzonitrile

Base Information

Chemical Name:4-(1-azido-2-iodoethyl)benzonitrile
CAS No.:1374152-36-9
Molecular Formula:C₉H₇IN₄
Molecular Weight:298.086
Hs Code.:

Synonyms:4-(1-azido-2-iodoethyl)benzonitrile

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Chemical Property of 4-(1-azido-2-iodoethyl)benzonitrile

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Technology Process of 4-(1-azido-2-iodoethyl)benzonitrile

There total 1 articles about 4-(1-azido-2-iodoethyl)benzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 3435-51-6
4-ethenylbenzonitrile

: 1374152-36-9
4-(1-azido-2-iodoethyl)benzonitrile

Guidance literature:: With sodium azide; [bis(acetoxy)iodo]benzene; iodine; In acetonitrile; at 25 ℃; for 1h;
DOI:10.1039/c6ob00532b

Reference yield:

: 1374152-36-9
4-(1-azido-2-iodoethyl)benzonitrile

: 623-26-7
terephthalonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / diethyl ether / 0 °C

2: bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]} / chloroform-d1 / 0.17 h / 25 °C / Inert atmosphere

With bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]}; potassium tert-butylate; In diethyl ether; chloroform-d1;
DOI:10.1002/anie.201801976

Reference yield:

: 1374152-36-9
4-(1-azido-2-iodoethyl)benzonitrile

: 623-26-7
terephthalonitrile

: benzyl (E)-5-(4-cyanophenyl)-2-(3-oxoprop-1-en-1-yl)-3,4-dihydro-2H-pyrrole-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / diethyl ether / 0 °C

2: dirhodium tetraacetate / dichloromethane / 16 h / 25 °C / Inert atmosphere

With dirhodium tetraacetate; potassium tert-butylate; In diethyl ether; dichloromethane;
DOI:10.1002/anie.201801976