3,3'-dibenzoyl-4,4'-dimethyl-2,2'-dipyrrolylmethane-5,5'-dicarboxylic acid

Base Information

Chemical Name:3,3'-dibenzoyl-4,4'-dimethyl-2,2'-dipyrrolylmethane-5,5'-dicarboxylic acid
CAS No.:858935-55-4
Molecular Formula:C₂₇H₂₂N₂O₆
Molecular Weight:470.481
Hs Code.:

Synonyms:3,3'-dibenzoyl-4,4'-dimethyl-2,2'-dipyrrolylmethane-5,5'-dicarboxylic acid

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Chemical Property of 3,3'-dibenzoyl-4,4'-dimethyl-2,2'-dipyrrolylmethane-5,5'-dicarboxylic acid

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Technology Process of 3,3'-dibenzoyl-4,4'-dimethyl-2,2'-dipyrrolylmethane-5,5'-dicarboxylic acid

There total 7 articles about 3,3'-dibenzoyl-4,4'-dimethyl-2,2'-dipyrrolylmethane-5,5'-dicarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 858935-77-0
dibenzyl 3,3'-dimethyl-4,4'-dibenzoyl-5,5'-dipyrrolylmethane-2,2'-dicarboxylate

: 858935-55-4
3,3'-dibenzoyl-4,4'-dimethyl-2,2'-dipyrrolylmethane-5,5'-dicarboxylic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1002/jhet.5570420405

Reference yield:

: 1201-93-0
1-phenyl-3-dimethylaminoprop-2-enone

: 858935-55-4
3,3'-dibenzoyl-4,4'-dimethyl-2,2'-dipyrrolylmethane-5,5'-dicarboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: Zn / acetic acid / 100 - 110 °C

2: 60 percent / LiN(Si(CH₃)3)2

3: 100 percent / BF₃*Et₂O / CH₂Cl₂

4: 99 percent / H₂ / Pd/C / tetrahydrofuran

With boron trifluoride diethyl etherate; hydrogen; lithium hexamethyldisilazane; zinc; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; acetic acid;
DOI:10.1002/jhet.5570420405

Reference yield:

: 858935-65-6
methyl 4-benzoyl-3-methylpyrrole-2-carboxylate

: 858935-55-4
3,3'-dibenzoyl-4,4'-dimethyl-2,2'-dipyrrolylmethane-5,5'-dicarboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / LiN(Si(CH₃)3)2

2: 100 percent / BF₃*Et₂O / CH₂Cl₂

3: 99 percent / H₂ / Pd/C / tetrahydrofuran

With boron trifluoride diethyl etherate; hydrogen; lithium hexamethyldisilazane; palladium on activated charcoal; In tetrahydrofuran; dichloromethane;
DOI:10.1002/jhet.5570420405