2-<4-<<<(4-chlorophenyl)amino>imino>methyl>phenoxy>-2-methylpropionic acid

Base Information

Chemical Name:2-<4-<<<(4-chlorophenyl)amino>imino>methyl>phenoxy>-2-methylpropionic acid
CAS No.:121809-59-4
Molecular Formula:C₁₇H₁₈ClN₃O₃
Molecular Weight:347.801
Hs Code.:

Synonyms:2-<4-<<<(4-chlorophenyl)amino>imino>methyl>phenoxy>-2-methylpropionic acid

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Chemical Property of 2-<4-<<<(4-chlorophenyl)amino>imino>methyl>phenoxy>-2-methylpropionic acid

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Technology Process of 2-<4-<<<(4-chlorophenyl)amino>imino>methyl>phenoxy>-2-methylpropionic acid

There total 6 articles about 2-<4-<<<(4-chlorophenyl)amino>imino>methyl>phenoxy>-2-methylpropionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 39536-21-5
S-methyl N-(4-chlorophenyl)amidino thioether

: 117011-70-8
2-(4-aminophenoxy)-2-methyl propionic acid

: 121809-59-4
2-<4-<<<(4-chlorophenyl)amino>imino>methyl>phenoxy>-2-methylpropionic acid

Guidance literature:: With piperidine; In isopropyl alcohol; for 24h; Heating;
DOI:10.1021/jm00130a021

Reference yield:

: 7159-95-7
(4-hydroxyphenyl)carbamic acid ethyl ester

: 121809-59-4
2-<4-<<<(4-chlorophenyl)amino>imino>methyl>phenoxy>-2-methylpropionic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 48 percent / NaOH / 4 h / Heating

2: 87 percent / 10percent KOH / 0.5 h / Heating

3: 72 percent / piperidine / propan-2-ol / 24 h / Heating

With piperidine; potassium hydroxide; sodium hydroxide; In isopropyl alcohol;
DOI:10.1021/jm00130a021

Reference yield:

: 767-00-0
4-cyanophenol

: 121809-59-4
2-<4-<<<(4-chlorophenyl)amino>imino>methyl>phenoxy>-2-methylpropionic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 78 percent / NaOH / a) 20 min, b) reflux, 4 h

2: 88 percent / 3percent H₂O₂, KOH / H₂O

3: 90 percent / Br₂, NaOH / H₂O / 0.5 h / 75 °C

4: 72 percent / piperidine / propan-2-ol / 24 h / Heating

With piperidine; potassium hydroxide; sodium hydroxide; dihydrogen peroxide; bromine; In water; isopropyl alcohol;
DOI:10.1021/jm00130a021