{3-[D₃]Methoxy-4-[2-(3,8,13-trimethoxy-7,12-bis{2-[2-methoxy-4-(tetrahydropyran-2-yloxymethyl)phenoxy]-[D₄]ethoxy}-10,15-dihydro-5H-tribenzo[a,d,g]cyclononen-2-yloxy)-[D₄]ethoxy]phenyl}methanol

Base Information

• Chemical Name: {3-[D₃]Methoxy-4-[2-(3,8,13-trimethoxy-7,12-bis{2-[2-methoxy-4-(tetrahydropyran-2-yloxymethyl)phenoxy]-[D₄]ethoxy}-10,15-dihydro-5H-tribenzo[a,d,g]cyclononen-2-yloxy)-[D₄]ethoxy]phenyl}methanol
• CAS No.: 347894-52-4
• Molecular Formula: C₆₄H₇₆O₁₇
• Molecular Weight: 1132.18

Synonyms:{3-[D₃]Methoxy-4-[2-(3,8,13-trimethoxy-7,12-bis{2-[2-methoxy-4-(tetrahydropyran-2-yloxymethyl)phenoxy]-[D₄]ethoxy}-10,15-dihydro-5H-tribenzo[a,d,g]cyclononen-2-yloxy)-[D₄]ethoxy]phenyl}methanol

Chemical Property of {3-[D₃]Methoxy-4-[2-(3,8,13-trimethoxy-7,12-bis{2-[2-methoxy-4-(tetrahydropyran-2-yloxymethyl)phenoxy]-[D₄]ethoxy}-10,15-dihydro-5H-tribenzo[a,d,g]cyclononen-2-yloxy)-[D₄]ethoxy]phenyl}methanol

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Technology Process of {3-[D₃]Methoxy-4-[2-(3,8,13-trimethoxy-7,12-bis{2-[2-methoxy-4-(tetrahydropyran-2-yloxymethyl)phenoxy]-[D₄]ethoxy}-10,15-dihydro-5H-tribenzo[a,d,g]cyclononen-2-yloxy)-[D₄]ethoxy]phenyl}methanol

There total 15 articles about {3-[D₃]Methoxy-4-[2-(3,8,13-trimethoxy-7,12-bis{2-[2-methoxy-4-(tetrahydropyran-2-yloxymethyl)phenoxy]-[D₄]ethoxy}-10,15-dihydro-5H-tribenzo[a,d,g]cyclononen-2-yloxy)-[D₄]ethoxy]phenyl}methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

2-[4-(2-[D4]Iodoethoxy)-3-methoxybenzyloxy]tetrahydropyran (347894-42-2) + 12-[2-(4-Hydroxymethyl-2-[D3]methoxyphenoxy)-[D4]ethoxy]-3,8,13-trimethoxy-10,15-dihydro-5H-tribenzo[a,d,g]cyclononene-2,7-diol (347894-50-2) → {3-[D3]Methoxy-4-[2-(3,8,13-trimethoxy-7,12-bis{2-[2-methoxy-4-(tetrahydropyran-2-yloxymethyl)phenoxy]-[D4]ethoxy}-10,15-dihydro-5H-tribenzo[a,d,g]cyclononen-2-yloxy)-[D4]ethoxy]phenyl}methanol (347894-52-4)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 18h;

DOI:10.1002/1521-3765(20010401)7:7<1561::AID-CHEM1561>3.0.CO;2-9

Reference yield:

3,4-dihydro-2H-pyran (110-87-2) → {3-[D3]Methoxy-4-[2-(3,8,13-trimethoxy-7,12-bis{2-[2-methoxy-4-(tetrahydropyran-2-yloxymethyl)phenoxy]-[D4]ethoxy}-10,15-dihydro-5H-tribenzo[a,d,g]cyclononen-2-yloxy)-[D4]ethoxy]phenyl}methanol (347894-52-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 83 percent / PPTS / tetrahydrofuran; CH₂Cl₂ / 20 °C

2: 95 percent / NaI / acetone / Heating

3: 78 percent / Cs₂CO₃ / dimethylformamide / 18 h / 80 °C

With pyridinium p-toluenesulfonate; caesium carbonate; sodium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetone;

DOI:10.1002/1521-3765(20010401)7:7<1561::AID-CHEM1561>3.0.CO;2-9

Reference yield:

4-hydroxymethyl-2-methoxyphenol (498-00-0) → {3-[D3]Methoxy-4-[2-(3,8,13-trimethoxy-7,12-bis{2-[2-methoxy-4-(tetrahydropyran-2-yloxymethyl)phenoxy]-[D4]ethoxy}-10,15-dihydro-5H-tribenzo[a,d,g]cyclononen-2-yloxy)-[D4]ethoxy]phenyl}methanol (347894-52-4)

Guidance literature:

Multi-step reaction with 4 steps

1: 48 percent / K₂CO₃ / acetone / 80 °C

2: 83 percent / PPTS / tetrahydrofuran; CH₂Cl₂ / 20 °C

3: 95 percent / NaI / acetone / Heating

4: 78 percent / Cs₂CO₃ / dimethylformamide / 18 h / 80 °C

With pyridinium p-toluenesulfonate; potassium carbonate; caesium carbonate; sodium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetone;

DOI:10.1002/1521-3765(20010401)7:7<1561::AID-CHEM1561>3.0.CO;2-9

upstream raw materials:

2-[4-(2-[D₄]Iodoethoxy)-3-methoxybenzyloxy]tetrahydropyran

12-[2-(4-Hydroxymethyl-2-[D₃]methoxyphenoxy)-[D₄]ethoxy]-3,8,13-trimethoxy-10,15-dihydro-5H-tribenzo[a,d,g]cyclononene-2,7-diol

3,4-dihydro-2H-pyran

4-hydroxymethyl-2-methoxyphenol

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